(S)-tert-butyl 1-(2-carbamoylphenylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

Base Information

Chemical Name:(S)-tert-butyl 1-(2-carbamoylphenylamino)-1-oxo-3-phenylpropan-2-ylcarbamate
CAS No.:1312716-40-7
Molecular Formula:C₂₁H₂₅N₃O₄
Molecular Weight:383.447
Hs Code.:

Synonyms:(S)-tert-butyl 1-(2-carbamoylphenylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

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Chemical Property of (S)-tert-butyl 1-(2-carbamoylphenylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

Chemical Property:

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Technology Process of (S)-tert-butyl 1-(2-carbamoylphenylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

There total 4 articles about (S)-tert-butyl 1-(2-carbamoylphenylamino)-1-oxo-3-phenylpropan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119153-87-6
(C₅H₉O₂)C₉H₉NO(O)(CO₂C₂H₅)

: 28144-70-9,88-68-6
anthranilic acid amide

: 1312716-40-7
(S)-tert-butyl 1-(2-carbamoylphenylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.01.009

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 1312716-40-7
(S)-tert-butyl 1-(2-carbamoylphenylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / tetrahydrofuran; water / 12 h / 0 - 20 °C

1.2: pH 2

2.1: triethylamine / tetrahydrofuran / 0.67 h / 0 °C / Inert atmosphere

3.1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With sodium carbonate; triethylamine; In tetrahydrofuran; water;
DOI:10.1016/j.tetasy.2011.01.009

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1312716-40-7
(S)-tert-butyl 1-(2-carbamoylphenylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 0.67 h / 0 °C / Inert atmosphere

2: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With triethylamine; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2011.01.009