N'-(4-nitrophenyl)hydrazine carboxylic acid butyl ester

Base Information

Chemical Name:N'-(4-nitrophenyl)hydrazine carboxylic acid butyl ester
CAS No.:42274-90-8
Molecular Formula:C₁₁H₁₅N₃O₄
Molecular Weight:253.258
Hs Code.:

Synonyms:N'-(4-nitrophenyl)hydrazine carboxylic acid butyl ester

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Chemical Property of N'-(4-nitrophenyl)hydrazine carboxylic acid butyl ester

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Technology Process of N'-(4-nitrophenyl)hydrazine carboxylic acid butyl ester

There total 3 articles about N'-(4-nitrophenyl)hydrazine carboxylic acid butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 109-65-9
1-bromo-butane

: 124-38-9,18923-20-1
carbon dioxide

: 100-16-3
4-nitrophenylhydrazone

: 42274-90-8
N'-(4-nitrophenyl)hydrazine carboxylic acid butyl ester

Guidance literature:: carbon dioxide; 4-nitrophenylhydrazone; In dimethyl sulfoxide; at 60 ℃; for 0.5h; Inert atmosphere;

With N-benzyl-trimethylammonium hydroxide; In dimethyl sulfoxide; at 60 ℃; for 0.5h; Inert atmosphere;

1-bromo-butane; In dimethyl sulfoxide; at 60 ℃; Inert atmosphere;
DOI:10.1007/s00706-008-0955-8

Reference yield: 85.0%

: 778-28-9
butyl para-toluenesulfonate

: 124-38-9,18923-20-1
carbon dioxide

: 100-16-3
4-nitrophenylhydrazone

: 42274-90-8
N'-(4-nitrophenyl)hydrazine carboxylic acid butyl ester

Guidance literature:: carbon dioxide; 4-nitrophenylhydrazone; With N-benzyl-trimethylammonium hydroxide; In dimethyl sulfoxide; at 60 ℃; for 0.5h; Inert atmosphere;

butyl para-toluenesulfonate; In dimethyl sulfoxide; at 60 ℃; for 4.5h; Inert atmosphere;
DOI:10.1080/00397910802269259

Reference yield: 82.0%

: 124-38-9,18923-20-1
carbon dioxide

: 100-16-3
4-nitrophenylhydrazone

: 71-36-3
butan-1-ol

: 42274-90-8
N'-(4-nitrophenyl)hydrazine carboxylic acid butyl ester

Guidance literature:: carbon dioxide; 4-nitrophenylhydrazone; In dimethyl sulfoxide; at 20 ℃; for 0.5h; Inert atmosphere;

butan-1-ol; With triphenylphosphine; diethylazodicarboxylate; In dimethyl sulfoxide; at 20 ℃; for 3.5h; chemoselective reaction; Inert atmosphere;
DOI:10.1007/BF03249073