2-(Benzenesulfonyl-methoxymethyl-amino)-3-(4-methoxymethoxy-phenyl)-propionic acid methoxymethyl ester

Base Information

Chemical Name:2-(Benzenesulfonyl-methoxymethyl-amino)-3-(4-methoxymethoxy-phenyl)-propionic acid methoxymethyl ester
CAS No.:184592-25-4
Molecular Formula:C₂₁H₂₇NO₈S
Molecular Weight:453.513
Hs Code.:

Synonyms:2-(Benzenesulfonyl-methoxymethyl-amino)-3-(4-methoxymethoxy-phenyl)-propionic acid methoxymethyl ester

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Chemical Property of 2-(Benzenesulfonyl-methoxymethyl-amino)-3-(4-methoxymethoxy-phenyl)-propionic acid methoxymethyl ester

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Technology Process of 2-(Benzenesulfonyl-methoxymethyl-amino)-3-(4-methoxymethoxy-phenyl)-propionic acid methoxymethyl ester

There total 4 articles about 2-(Benzenesulfonyl-methoxymethyl-amino)-3-(4-methoxymethoxy-phenyl)-propionic acid methoxymethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 184759-46-4
N-(phenylsulfonyl)-DL-tyrosine

: 107-30-2
chloromethyl methyl ether

: 184592-25-4
2-(Benzenesulfonyl-methoxymethyl-amino)-3-(4-methoxymethoxy-phenyl)-propionic acid methoxymethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 0 ℃; for 1.5h;
DOI:10.1021/jm960581w

Reference yield:

: 3417-91-2,3728-20-9,68697-61-0
tyrosine methyl ester hydrochloride

: 184592-25-4
2-(Benzenesulfonyl-methoxymethyl-amino)-3-(4-methoxymethoxy-phenyl)-propionic acid methoxymethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / 1 N NaOH / CH₂Cl₂ / 2 h

2: 100 percent / aq. KOH / ethanol / 48 h / 60 °C

3: 46 percent / N,N-diisopropylethylamine / acetonitrile / 1.5 h / 0 °C

With potassium hydroxide; sodium hydroxide; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jm960581w

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 184592-25-4
2-(Benzenesulfonyl-methoxymethyl-amino)-3-(4-methoxymethoxy-phenyl)-propionic acid methoxymethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / 1 N NaOH / CH₂Cl₂ / 2 h

2: 100 percent / aq. KOH / ethanol / 48 h / 60 °C

3: 46 percent / N,N-diisopropylethylamine / acetonitrile / 1.5 h / 0 °C

With potassium hydroxide; sodium hydroxide; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jm960581w