ethyl 6-(4-methoxybenzyl)-4-hydroxy-2-oxo-1,2-dihydropyridine-3-carboxylate

Base Information

Chemical Name:ethyl 6-(4-methoxybenzyl)-4-hydroxy-2-oxo-1,2-dihydropyridine-3-carboxylate
CAS No.:1430414-45-1
Molecular Formula:C₁₆H₁₇NO₅
Molecular Weight:303.315
Hs Code.:

Synonyms:ethyl 6-(4-methoxybenzyl)-4-hydroxy-2-oxo-1,2-dihydropyridine-3-carboxylate

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Chemical Property of ethyl 6-(4-methoxybenzyl)-4-hydroxy-2-oxo-1,2-dihydropyridine-3-carboxylate

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Technology Process of ethyl 6-(4-methoxybenzyl)-4-hydroxy-2-oxo-1,2-dihydropyridine-3-carboxylate

There total 4 articles about ethyl 6-(4-methoxybenzyl)-4-hydroxy-2-oxo-1,2-dihydropyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: C₁₃H₁₇NO₃

: 105-53-3
diethyl malonate

: 1430414-45-1
ethyl 6-(4-methoxybenzyl)-4-hydroxy-2-oxo-1,2-dihydropyridine-3-carboxylate

Guidance literature:: diethyl malonate; With sodium; In ethanol; for 1h;

C₁₃H₁₇NO₃; In ethanol; for 96h; Reflux;
DOI:10.1021/jm400102x

Reference yield:

: 32711-91-4
ethyl 4-(4-methoxylphenyl)-3-oxobutanoate

: 1430414-45-1
ethyl 6-(4-methoxybenzyl)-4-hydroxy-2-oxo-1,2-dihydropyridine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonia / methanol / 8 h / Reflux; Sealed tube

2.1: sodium / ethanol / 1 h

2.2: 96 h / Reflux

With ammonia; sodium; In methanol; ethanol;
DOI:10.1021/jm400102x

Reference yield:

: 226956-10-1
5-[2-(4-Methoxy-phenyl)-acetyl]-2,2-dimethyl-[1,3]dioxane-4,6-dione

: 1430414-45-1
ethyl 6-(4-methoxybenzyl)-4-hydroxy-2-oxo-1,2-dihydropyridine-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4 h / Reflux

2.1: ammonia / methanol / 8 h / Reflux; Sealed tube

3.1: sodium / ethanol / 1 h

3.2: 96 h / Reflux

With ammonia; sodium; In methanol; ethanol;
DOI:10.1021/jm400102x