D-Lysine, N2-[(1,1-dimethylethoxy)carbonyl]-N6-[(phenylmethoxy)carbonyl]-, methyl ester

Base Information

Chemical Name:D-Lysine, N2-[(1,1-dimethylethoxy)carbonyl]-N6-[(phenylmethoxy)carbonyl]-, methyl ester
CAS No.:82611-49-2
Molecular Formula:C₂₀H₃₀N₂O₆
Molecular Weight:394.468
Hs Code.:
Mol file:82611-49-2.mol

Synonyms:methyl 6-N-benzyloxycarbonyl-2-N-BOC-D-lysinate

Suppliers and Price of D-Lysine, N2-[(1,1-dimethylethoxy)carbonyl]-N6-[(phenylmethoxy)carbonyl]-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of D-Lysine, N2-[(1,1-dimethylethoxy)carbonyl]-N6-[(phenylmethoxy)carbonyl]-, methyl ester

Chemical Property:

Vapor Pressure:0mmHg at 25°C

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of D-Lysine, N2-[(1,1-dimethylethoxy)carbonyl]-N6-[(phenylmethoxy)carbonyl]-, methyl ester

There total 4 articles about D-Lysine, N2-[(1,1-dimethylethoxy)carbonyl]-N6-[(phenylmethoxy)carbonyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 55878-47-2
(R)-6-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-hexanoic acid

: 74-88-4
methyl iodide

: 82611-49-2
methyl 6-N-benzyloxycarbonyl-2-N-BOC-D-lysinate

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 36h;
DOI:10.3184/174751915X14326563172262

Reference yield:

: 923-27-3,3506-25-0
D-lysine

: 82611-49-2
methyl 6-N-benzyloxycarbonyl-2-N-BOC-D-lysinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(II) sulfate; sodium hydroxide / water / 5 h / 20 °C

1.2: 3 h / 20 °C

2.1: sodium hydroxide / water; 1,4-dioxane / 14 h / 20 °C

3.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 36 h / 20 °C

With sodium hydrogencarbonate; copper(II) sulfate; sodium hydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.3184/174751915X14326563172262

Reference yield:

: 34404-32-5,1155-64-2,32302-83-3,57705-97-2,67178-46-5,25931-47-9
(R)-2-amino-6-(((benzyloxy)carbonyl)amino)hexanoic acid

: 82611-49-2
methyl 6-N-benzyloxycarbonyl-2-N-BOC-D-lysinate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water; 1,4-dioxane / 14 h / 20 °C

2: sodium hydrogencarbonate / N,N-dimethyl-formamide / 36 h / 20 °C

With sodium hydrogencarbonate; sodium hydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.3184/174751915X14326563172262