C₄₂H₃₈N₂O₅

Base Information

Chemical Name:C₄₂H₃₈N₂O₅
CAS No.:1384461-41-9
Molecular Formula:C₄₂H₃₈N₂O₅
Molecular Weight:650.774
Hs Code.:

C<sub>42</sub>H<sub>38</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₄₂H₃₈N₂O₅

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Chemical Property of C₄₂H₃₈N₂O₅

Chemical Property:

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Technology Process of C₄₂H₃₈N₂O₅

There total 9 articles about C₄₂H₃₈N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1384461-34-0
2-amino-1-(6,8-bis(benzyloxy)-1-vinyl-3,4-dihydroisoquinolin-2(1H)-yl)ethanone

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1384461-41-9
C₄₂H₃₈N₂O₅

Guidance literature:: With triethylamine; In dichloromethane; Inert atmosphere;
DOI:10.1039/c2ob25772f

Reference yield:

: 1384461-36-2
C₂₆H₂₇NO₂

: 1384461-41-9
C₄₂H₃₈N₂O₅

Guidance literature:: Multi-step reaction with 7 steps

1: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 12 h / Inert atmosphere

2: sodium periodate / tetrahydrofuran; water / 0.33 h / Inert atmosphere

3: sodium tetrahydroborate / methanol / 0.08 h / Inert atmosphere

4: tributylphosphine / tetrahydrofuran / 4 h / Inert atmosphere

5: dihydrogen peroxide / tetrahydrofuran / 6 h / 45 °C / Inert atmosphere

6: triphenylphosphine / tetrahydrofuran; water / 12 h / Inert atmosphere

7: triethylamine / dichloromethane / Inert atmosphere

With dmap; sodium tetrahydroborate; sodium periodate; tributylphosphine; dihydrogen peroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c2ob25772f

Reference yield:

: 1384461-35-1
6,8-bis(benzyloxy)-3,4-dihydroisoquinoline

: 1384461-41-9
C₄₂H₃₈N₂O₅

Guidance literature:: Multi-step reaction with 8 steps

1: tetrahydrofuran / 5 h / -78 - 0 °C / Inert atmosphere

2: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 12 h / Inert atmosphere

3: sodium periodate / tetrahydrofuran; water / 0.33 h / Inert atmosphere

4: sodium tetrahydroborate / methanol / 0.08 h / Inert atmosphere

5: tributylphosphine / tetrahydrofuran / 4 h / Inert atmosphere

6: dihydrogen peroxide / tetrahydrofuran / 6 h / 45 °C / Inert atmosphere

7: triphenylphosphine / tetrahydrofuran; water / 12 h / Inert atmosphere

8: triethylamine / dichloromethane / Inert atmosphere

With dmap; sodium tetrahydroborate; sodium periodate; tributylphosphine; dihydrogen peroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c2ob25772f