5-Iodo-1,3,6-trimethylpyrimidine-2,4(1H,3H)-dione

Base Information

Chemical Name:5-Iodo-1,3,6-trimethylpyrimidine-2,4(1H,3H)-dione
CAS No.:134039-54-6
Molecular Formula:C7H9IN2O2
Molecular Weight:280.065
Hs Code.:2933599090
DSSTox Substance ID:DTXSID40448543
Nikkaji Number:J396.840E
Mol file:134039-54-6.mol

Synonyms:134039-54-6;5-iodo-1,3,6-trimethylpyrimidine-2,4-dione;5-Iodo-1,3,6-trimethylpyrimidine-2,4(1H,3H)-dione;5-Iodo-1,3,6-trimethyluracil;2,4(1H,3H)-Pyrimidinedione,5-iodo-1,3,6-trimethyl-;SCHEMBL1689679;5-iodo-1,3,6-trimethyl uracil;DTXSID40448543;OGGRCIQVWZBFPS-UHFFFAOYSA-N;AKOS015908977

Suppliers and Price of 5-Iodo-1,3,6-trimethylpyrimidine-2,4(1H,3H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-IODO-1,3,6-TRIMETHYLURACIL 95.00%
5MG
$ 497.00

Total 8 raw suppliers

Chemical Property of 5-Iodo-1,3,6-trimethylpyrimidine-2,4(1H,3H)-dione

Chemical Property:

Vapor Pressure:0.006mmHg at 25°C
Melting Point:152-153 °C(Solv: ligroine (8032-32-4))
Refractive Index:1.64
Boiling Point:273.01 °C at 760 mmHg
PKA:-3.51±0.60(Predicted)
Flash Point:118.912 °C
PSA：44.00000
Density:1.91 g/cm³
LogP:-0.00300
XLogP3:0.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:279.97088
Heavy Atom Count:12
Complexity:285

Purity/Quality:

98%min ^*data from raw suppliers

5-IODO-1,3,6-TRIMETHYLURACIL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=O)N(C(=O)N1C)C)I

Technology Process of 5-Iodo-1,3,6-trimethylpyrimidine-2,4(1H,3H)-dione

There total 2 articles about 5-Iodo-1,3,6-trimethylpyrimidine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 13509-52-9
1,3,6-trimethyluracil

: 134039-54-6
1,2,3,4-Tetrahydro-5-iodo-1,3,6-trimethyl-2,4-dioxopyrimidine

Guidance literature:: With sulfuric acid; dihydrogen peroxide; potassium iodide; at 20 - 25 ℃;
DOI:10.1007/s11172-013-0354-0

Reference yield: 93.0%

: 1461-67-2
5-iodine-6-methyl-1H-pyrimidine-2,4-dione

: 74-88-4
methyl iodide

: 134039-54-6
1,2,3,4-Tetrahydro-5-iodo-1,3,6-trimethyl-2,4-dioxopyrimidine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide;

Reference yield: 72.0%

: 134039-54-6
1,2,3,4-Tetrahydro-5-iodo-1,3,6-trimethyl-2,4-dioxopyrimidine

: 113850-76-3,210962-91-7
N-(tert-butoxycarbonyl)-4-iodo-L-phenylalanine methyl ester

: 343850-60-2
(S)-2-tert-butoxycarbonylamino-3-[4-(1,3,6-trimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)phenyl]propionic acid methyl ester

Guidance literature:: 1,2,3,4-Tetrahydro-5-iodo-1,3,6-trimethyl-2,4-dioxopyrimidine; With chloro-trimethyl-silane; zinc; In tetrahydrofuran; dimethyl amine; ethylene dibromide; at 20 - 70 ℃;

N-(tert-butoxycarbonyl)-4-iodo-L-phenylalanine methyl ester; With tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; at 50 - 55 ℃; for 48h;