(Z)-methyl 4-amino-α-<<(tetrahydro-2H-pyran-2-yl)-oxy>imino>phenylacetate

Base Information

Chemical Name:(Z)-methyl 4-amino-α-<<(tetrahydro-2H-pyran-2-yl)-oxy>imino>phenylacetate
CAS No.:75626-60-7
Molecular Formula:C₁₄H₁₈N₂O₄
Molecular Weight:278.308
Hs Code.:

Synonyms:(Z)-methyl 4-amino-α-<<(tetrahydro-2H-pyran-2-yl)-oxy>imino>phenylacetate

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Chemical Property of (Z)-methyl 4-amino-α-<<(tetrahydro-2H-pyran-2-yl)-oxy>imino>phenylacetate

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Technology Process of (Z)-methyl 4-amino-α-<<(tetrahydro-2H-pyran-2-yl)-oxy>imino>phenylacetate

There total 8 articles about (Z)-methyl 4-amino-α-<<(tetrahydro-2H-pyran-2-yl)-oxy>imino>phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75626-59-4
(4-Benzyloxycarbonylamino-phenyl)-[(Z)-tetrahydro-pyran-2-yloxyimino]-acetic acid methyl ester

: 75626-60-7
(Z)-methyl 4-amino-α-<<(tetrahydro-2H-pyran-2-yl)-oxy>imino>phenylacetate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 0.5h;
DOI:10.1021/jo00314a029

Reference yield:

: 72531-10-3
4-<<(benzyloxy)carbonyl>amino>acetophenone

: 75626-60-7
(Z)-methyl 4-amino-α-<<(tetrahydro-2H-pyran-2-yl)-oxy>imino>phenylacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / selenium dioxide / 3 h / 100 °C

2: 59 percent / pyridine / 4 h / 0 °C

3: 98 percent / methanol; diethyl ether / 0 °C

4: 100 percent / H₂ / palladium on carbon / ethyl acetate / 0.5 h

With selenium(IV) oxide; hydrogen; palladium on activated charcoal; In pyridine; methanol; diethyl ether; ethyl acetate;
DOI:10.1021/jo00314a029

Reference yield:

: 75626-51-6
4-<<(benzyloxy)carbonyl>amino>-α-oxophenylacetic acid

: 75626-60-7
(Z)-methyl 4-amino-α-<<(tetrahydro-2H-pyran-2-yl)-oxy>imino>phenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / pyridine / 4 h / 0 °C

2: 98 percent / methanol; diethyl ether / 0 °C

3: 100 percent / H₂ / palladium on carbon / ethyl acetate / 0.5 h

With hydrogen; palladium on activated charcoal; In pyridine; methanol; diethyl ether; ethyl acetate;
DOI:10.1021/jo00314a029