N-<3(RS)--1-oxo-2-benzylpropyl>glycine isopentylamide

Base Information

Chemical Name:N-<3(RS)--1-oxo-2-benzylpropyl>glycine isopentylamide
CAS No.:96866-18-1
Molecular Formula:C₂₅H₃₃N₃O₄
Molecular Weight:439.555
Hs Code.:

N-<3(RS)-<N-(benzyloxy)-N-formylamino>-1-oxo-2-benzylpropyl>glycine isopentylamide

Synonyms:N-<3(RS)--1-oxo-2-benzylpropyl>glycine isopentylamide

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Chemical Property of N-<3(RS)--1-oxo-2-benzylpropyl>glycine isopentylamide

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Technology Process of N-<3(RS)--1-oxo-2-benzylpropyl>glycine isopentylamide

There total 5 articles about N-<3(RS)--1-oxo-2-benzylpropyl>glycine isopentylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 84851-16-1
N-(tert-butyloxycarbonyl)glycine isopentylamide

: 96866-15-8
3(RS)--2-benzylpropanoic acid

: 96866-18-1
N-<3(RS)--1-oxo-2-benzylpropyl>glycine isopentylamide

Guidance literature:: With N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; benzotriazol-1-ol; triethylamine; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jm00147a007

Reference yield:

: 107-85-7
1-amino-3-methylbutane

: 96866-18-1
N-<3(RS)--1-oxo-2-benzylpropyl>glycine isopentylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

2: 80 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), N-cyclohexyl-N'-<2-(4-morpholinyl)ethyl>carbodiimide methol p-toluenosulfonate / tetrahydrofuran / Ambient temperature

With N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; chloroform;
DOI:10.1021/jm00147a007

Reference yield:

: 5669-19-2
2-Benzyl-2-propenoic acid

: 96866-18-1
N-<3(RS)--1-oxo-2-benzylpropyl>glycine isopentylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / ethanol / 168 h / Heating

2: 98 percent / acetic anhydride / 3 h / 0 °C

3: 80 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), N-cyclohexyl-N'-<2-(4-morpholinyl)ethyl>carbodiimide methol p-toluenosulfonate / tetrahydrofuran / Ambient temperature

With acetic anhydride; N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; benzotriazol-1-ol; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00147a007