Cyclohexyl benzenesulphonate

Base Information

• Chemical Name: Cyclohexyl benzenesulphonate
• CAS No.: 782-84-3
• Molecular Formula: C₁₂H₁₆O₃S
• Molecular Weight: 240.323
• Mol file: 782-84-3.mol

Synonyms:Cyclohexyl benzenesulphonate

Chemical Property of Cyclohexyl benzenesulphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cyclohexyl benzenesulphonate

There total 4 articles about Cyclohexyl benzenesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

benzenesulfonic acid (98-11-3) + cyclohexanol (108-93-0) → Cyclohexyl benzenesulphonate (782-84-3)

Guidance literature:

Fe⁽³⁺⁾-exchanged montmorillonite clay; In 1,2-dichloro-ethane; at 80 ℃; for 4h;

DOI:10.1016/S0040-4020(00)00626-8

Reference yield: 77.0%

2-(cyclohexyloxy)tetrahydro-2H-pyran (709-83-1) + benzenesulfonyl chloride (98-09-9) → Cyclohexyl benzenesulphonate (782-84-3)

Guidance literature:

With FeCl₃-Montmorillonite K-10; In acetonitrile; for 8h; Heating;

DOI:10.1515/znb-2005-0711

Reference yield: 71.0%

benzenesulfonyl chloride (98-09-9) + cyclohexanol (108-93-0) → Cyclohexyl benzenesulphonate (782-84-3)

Guidance literature:

With cesium fluoride supported on Celite; at 50 ℃; for 2.5h; chemoselective reaction;

DOI:10.1016/j.catcom.2011.04.005

upstream raw materials:

benzenesulfonyl chloride

cyclohexanol

benzenesulfonic acid

cyclohexene

Downstream raw materials:

2-cyclohexyl-fluorene

(4-cyclohexyl-phenyl)-phenyl-methane

9-cyclohexyl-phenanthrene

2-cyclohexyl-phenanthrene

Refernces

• 1、 Movassagh, Barahman,Shokri, Salman. "An efficient one-pot conversion of THP and TMS ethers to sulfonate esters using FeCl3-montmorillonite K-10 clay". . p. 763 - 765. Retrieved 2007/10/03.
• 2、 Bates, Gordon S.,Ramaswamy, S.. "2,2-Bis(ethylthio)ethanenitrile: preparation and use as a one or two carbon nucleophile". . p. 2006 - 2009. Retrieved 2007/10/02.