1-tert-butyl 4-ethyl 4-((4-nitrophenyl)sulfanyl)piperidine-1,4-dicarboxylate

Base Information

Chemical Name:1-tert-butyl 4-ethyl 4-((4-nitrophenyl)sulfanyl)piperidine-1,4-dicarboxylate
CAS No.:1438386-11-8
Molecular Formula:C₁₉H₂₆N₂O₆S
Molecular Weight:410.491
Hs Code.:

Synonyms:1-tert-butyl 4-ethyl 4-((4-nitrophenyl)sulfanyl)piperidine-1,4-dicarboxylate

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Chemical Property of 1-tert-butyl 4-ethyl 4-((4-nitrophenyl)sulfanyl)piperidine-1,4-dicarboxylate

Chemical Property:

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Technology Process of 1-tert-butyl 4-ethyl 4-((4-nitrophenyl)sulfanyl)piperidine-1,4-dicarboxylate

There total 3 articles about 1-tert-butyl 4-ethyl 4-((4-nitrophenyl)sulfanyl)piperidine-1,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 100-32-3
di(p-nitrophenyl) disulfide

: 142851-03-4
1-tert-butyl 4-ethyl piperidine-1,4-dicarboxylate

: 1438386-11-8
1-tert-butyl 4-ethyl 4-((4-nitrophenyl)sulfanyl)piperidine-1,4-dicarboxylate

Guidance literature:: 1-tert-butyl 4-ethyl piperidine-1,4-dicarboxylate; With lithium diisopropyl amide; In tetrahydrofuran; at -78 - 0 ℃; for 1h; Inert atmosphere;

di(p-nitrophenyl) disulfide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c3ob41046c

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1438386-11-8
1-tert-butyl 4-ethyl 4-((4-nitrophenyl)sulfanyl)piperidine-1,4-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine / acetonitrile

2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 - 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With iodine; lithium diisopropyl amide; In tetrahydrofuran; acetonitrile;
DOI:10.1039/c3ob41046c

Reference yield:

: 1126-09-6
4-carbethoxypiperidine

: 1438386-11-8
1-tert-butyl 4-ethyl 4-((4-nitrophenyl)sulfanyl)piperidine-1,4-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine / acetonitrile

2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 - 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With iodine; lithium diisopropyl amide; In tetrahydrofuran; acetonitrile;
DOI:10.1039/c3ob41046c