3-[2-(Ethoxycarbonyl)ethyl]benzeneboronic acid pinacol ester, 97%

Base Information

Chemical Name:3-[2-(Ethoxycarbonyl)ethyl]benzeneboronic acid pinacol ester, 97%
CAS No.:935854-36-7
Molecular Formula:C₁₇H₂₅BO₄
Molecular Weight:304.194
Hs Code.:
Mol file:935854-36-7.mol

Synonyms:ethyl 3-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-propionate

Suppliers and Price of 3-[2-(Ethoxycarbonyl)ethyl]benzeneboronic acid pinacol ester, 97%

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alfa Aesar
3-[2-(Ethoxycarbonyl)ethyl]benzeneboronic acid pinacol ester 97%
5g
$ 160.00

Alfa Aesar
3-[2-(Ethoxycarbonyl)ethyl]benzeneboronic acid pinacol ester 97%
1g
$ 60.40

Total 5 raw suppliers

Chemical Property of 3-[2-(Ethoxycarbonyl)ethyl]benzeneboronic acid pinacol ester, 97%

Chemical Property:

Water Solubility.:Insoluble in water

Purity/Quality:

99%,98%, ^*data from raw suppliers

3-[2-(Ethoxycarbonyl)ethyl]benzeneboronic acid pinacol ester 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-[2-(Ethoxycarbonyl)ethyl]benzeneboronic acid pinacol ester, 97%

There total 3 articles about 3-[2-(Ethoxycarbonyl)ethyl]benzeneboronic acid pinacol ester, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 40640-97-9
ethyl 3-(3-bromophenyl)propanoate

: 73183-34-3
bis(pinacol)diborane

: 935854-36-7
ethyl 3-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-propionate

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 80 - 85 ℃; for 8h; Inert atmosphere;

Reference yield: 97.0%

: 935854-36-7
ethyl 3-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-propionate

Guidance literature:

Reference yield:

: 42287-90-1
3-(3-bromophenyl)propanoic acid

: 935854-36-7
ethyl 3-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-propionate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 80 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; thionyl chloride; potassium acetate; In 1,4-dioxane;
DOI:10.1016/j.bmcl.2011.01.024