chloro(N,N'-diphenyl-1,8-diamidonaphthalene)stibine

Base Information

Chemical Name:chloro(N,N'-diphenyl-1,8-diamidonaphthalene)stibine
CAS No.:952064-63-0
Molecular Formula:C₂₂H₁₆ClN₂Sb
Molecular Weight:465.585
Hs Code.:

Synonyms:chloro(N,N'-diphenyl-1,8-diamidonaphthalene)stibine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of chloro(N,N'-diphenyl-1,8-diamidonaphthalene)stibine

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Technology Process of chloro(N,N'-diphenyl-1,8-diamidonaphthalene)stibine

There total 1 articles about chloro(N,N'-diphenyl-1,8-diamidonaphthalene)stibine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 10025-91-9
antimony(III) chloride

: 138052-77-4
N,N'-diphenyl-1,8-diaminonaphthalene

: 952064-63-0
chloro(N,N'-diphenyl-1,8-diamidonaphthalene)stibine

Guidance literature:: With triethyl amine; In toluene; (N2; Schlenk or glovebox) to a soln. of diaminonaphthalene in toluene was added sequentially 1 equiv of SbCl3 followed by N(C2H5)3 (2.6 equiv), the mixt. was stirred for 4 days; volatiles were removed under vac., toluene was added, filtered through aglass frit packed with Celite, volatiles were removed, the solid was re crystd. from 50:50 toluene/hexane mixt. at -20°C overnight; elem.anal.;
DOI:10.1021/om7004436

Reference yield:

: 952064-63-0
chloro(N,N'-diphenyl-1,8-diamidonaphthalene)stibine

: 7440-36-0
antimony

Guidance literature:: With GaCl₃ or AlCl₃; In toluene; (N2, Schlenk or glovebox) addn. of GaCl3 or AlCl3 to toluene soln. at low temp.;
DOI:10.1021/om7004436