(1R,3R,4R)-3-[4-(1',1'-dimethylheptyl)-2,6-dihydroxyphenyl]-4-isopropenyl-1-methoxycarbonylcyclohexane

Base Information

Chemical Name:(1R,3R,4R)-3-[4-(1',1'-dimethylheptyl)-2,6-dihydroxyphenyl]-4-isopropenyl-1-methoxycarbonylcyclohexane
CAS No.:1605280-83-8
Molecular Formula:C₂₆H₄₀O₄
Molecular Weight:416.601
Hs Code.:

Synonyms:(1R,3R,4R)-3-[4-(1',1'-dimethylheptyl)-2,6-dihydroxyphenyl]-4-isopropenyl-1-methoxycarbonylcyclohexane

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Chemical Property of (1R,3R,4R)-3-[4-(1',1'-dimethylheptyl)-2,6-dihydroxyphenyl]-4-isopropenyl-1-methoxycarbonylcyclohexane

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Technology Process of (1R,3R,4R)-3-[4-(1',1'-dimethylheptyl)-2,6-dihydroxyphenyl]-4-isopropenyl-1-methoxycarbonylcyclohexane

There total 3 articles about (1R,3R,4R)-3-[4-(1',1'-dimethylheptyl)-2,6-dihydroxyphenyl]-4-isopropenyl-1-methoxycarbonylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1605280-80-5
(1R,3R,4R)-3-[4-(1',1'-dimethylheptyl)-2,6-dihydroxyphenyl]-4-isopropenyl-1-carboxylylcyclohexane

: 18107-18-1
diazomethyl-trimethyl-silane

: 1605280-83-8
(1R,3R,4R)-3-[4-(1',1'-dimethylheptyl)-2,6-dihydroxyphenyl]-4-isopropenyl-1-methoxycarbonylcyclohexane

: 1605280-84-9
(1R,3R,4R)-methyl 3-(2-hydroxy-6-methoxy-4-(2-methyloctan-2-yl)phenyl)-4-(prop-1-en-2-yl)cyclohexanecarboxylate

Guidance literature:: In methanol; toluene; at 0 - 20 ℃;

Reference yield:

: 213915-75-4
(1R,3R,4R)-3-[2,6-Bis-(tert-butyl-dimethyl-silanyloxy)-4-(1,1-dimethyl-heptyl)-phenyl]-4-isopropenyl-cyclohexanecarbaldehyde

: 1605280-83-8
(1R,3R,4R)-3-[4-(1',1'-dimethylheptyl)-2,6-dihydroxyphenyl]-4-isopropenyl-1-methoxycarbonylcyclohexane

: 1605280-84-9
(1R,3R,4R)-methyl 3-(2-hydroxy-6-methoxy-4-(2-methyloctan-2-yl)phenyl)-4-(prop-1-en-2-yl)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium dihydrogenphosphate / tert-butyl alcohol; water / 0.17 h / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C

3: toluene; methanol / 0 - 20 °C

With sodium dihydrogenphosphate; tetrabutyl ammonium fluoride; In tetrahydrofuran; methanol; water; toluene; tert-butyl alcohol;

Reference yield:

: 1605281-26-2
(1R,3R,4R)-3-[4-(1',1'-dimethylheptyl)-2,6-bis(tert-butyldimethylsilyloxy)phenyl]-4-isopropenyl-1-carboxylcyclohexane

: 1605280-83-8
(1R,3R,4R)-3-[4-(1',1'-dimethylheptyl)-2,6-dihydroxyphenyl]-4-isopropenyl-1-methoxycarbonylcyclohexane

: 1605280-84-9
(1R,3R,4R)-methyl 3-(2-hydroxy-6-methoxy-4-(2-methyloctan-2-yl)phenyl)-4-(prop-1-en-2-yl)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C

2: toluene; methanol / 0 - 20 °C

With tetrabutyl ammonium fluoride; In tetrahydrofuran; methanol; toluene;