[(E)-(1S)-1-((1R)-3,3-dibromo-1-methylallyl)-5-(4-methoxybenzyloxy)pent-2-enyloxy]triisopropylsilane

Base Information

Chemical Name:[(E)-(1S)-1-((1R)-3,3-dibromo-1-methylallyl)-5-(4-methoxybenzyloxy)pent-2-enyloxy]triisopropylsilane
CAS No.:1071956-48-3
Molecular Formula:C₂₆H₄₂Br₂O₃Si
Molecular Weight:590.511
Hs Code.:

Synonyms:[(E)-(1S)-1-((1R)-3,3-dibromo-1-methylallyl)-5-(4-methoxybenzyloxy)pent-2-enyloxy]triisopropylsilane

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Chemical Property of [(E)-(1S)-1-((1R)-3,3-dibromo-1-methylallyl)-5-(4-methoxybenzyloxy)pent-2-enyloxy]triisopropylsilane

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Technology Process of [(E)-(1S)-1-((1R)-3,3-dibromo-1-methylallyl)-5-(4-methoxybenzyloxy)pent-2-enyloxy]triisopropylsilane

There total 1 articles about [(E)-(1S)-1-((1R)-3,3-dibromo-1-methylallyl)-5-(4-methoxybenzyloxy)pent-2-enyloxy]triisopropylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 558-13-4
carbon tetrabromide

: 1071956-66-5
(E)-(2S,3S)-7-(4-methoxybenzyloxy)-2-methyl-3-trisopropylsilanyloxyhept-4-enal

: 1071956-48-3
[(E)-(1S)-1-((1R)-3,3-dibromo-1-methylallyl)-5-(4-methoxybenzyloxy)pent-2-enyloxy]triisopropylsilane

Guidance literature:: carbon tetrabromide; With triphenylphosphine; zinc; In dichloromethane; at 0 - 20 ℃; for 0.5h;

(E)-(2S,3S)-7-(4-methoxybenzyloxy)-2-methyl-3-trisopropylsilanyloxyhept-4-enal; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ol801708x

Reference yield: 87.0%

: 75-77-4
chloro-trimethyl-silane

: 1071956-48-3
[(E)-(1S)-1-((1R)-3,3-dibromo-1-methylallyl)-5-(4-methoxybenzyloxy)pent-2-enyloxy]triisopropylsilane

: 1071956-50-7
1-methoxy-4-((E)-(5S,6R)-6-methyl-5-triisopropylsilanyloxy-8-trimethylsilanyloct-3-en-7-ynyloxymethyl)benzene

Guidance literature:: [(E)-(1S)-1-((1R)-3,3-dibromo-1-methylallyl)-5-(4-methoxybenzyloxy)pent-2-enyloxy]triisopropylsilane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3h;
DOI:10.1021/ol801708x