2-(4-Methoxybenzyl)-1,3-dithiane

Base Information

Chemical Name:2-(4-Methoxybenzyl)-1,3-dithiane
CAS No.:74447-45-3
Molecular Formula:C₁₂H₁₆OS₂
Molecular Weight:240.39
Hs Code.:
DSSTox Substance ID:DTXSID601273797
Nikkaji Number:J724.855E

Synonyms:2-(4-Methoxybenzyl)-1,3-dithiane;2-[(4-methoxyphenyl)methyl]-1,3-dithiane;74447-45-3;DTXSID601273797;AKOS024322327;2-(4-METHOXY-BENZYL)-(1,3)DITHIANE

Suppliers and Price of 2-(4-Methoxybenzyl)-1,3-dithiane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-Methoxybenzyl)-1,3-dithiane

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:240.06425748
Heavy Atom Count:15
Complexity:173

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)CC2SCCCS2

Technology Process of 2-(4-Methoxybenzyl)-1,3-dithiane

There total 2 articles about 2-(4-Methoxybenzyl)-1,3-dithiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 109-80-8
1.3-propanedithiol

: 5703-26-4
4-Methoxyphenylacetaldehyde

: 74447-45-3
2-(4-methoxyphenyl)methyl-1,3-dithiane

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; Molecular sieve;
DOI:10.1016/j.tet.2010.12.001

Reference yield: 54.0%

: 505-23-7
1,3 dithiane

: 824-94-2
p-methoxybenzyl chloride

: 74447-45-3
2-(4-methoxyphenyl)methyl-1,3-dithiane

Guidance literature:: 1,3 dithiane; With n-butyllithium; In tetrahydrofuran; hexane; for 1.33333h; Inert atmosphere; Glovebox; Cooling with acetone-dry ice;

p-methoxybenzyl chloride; In tetrahydrofuran; hexane; at 0 - 20 ℃; Inert atmosphere; Glovebox;
DOI:10.1021/acs.joc.5b00547

Reference yield: 87.0%

: 74447-45-3
2-(4-methoxyphenyl)methyl-1,3-dithiane

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1268631-74-8
2-(4-methoxybenzyl)-1,3-dithiane-2-carbaldehyde

Guidance literature:: 2-(4-methoxyphenyl)methyl-1,3-dithiane; With n-butyllithium; In tetrahydrofuran; at -20 ℃; for 0.5h;

N,N-dimethyl-formamide; In tetrahydrofuran; at 20 ℃; for 6h;
DOI:10.3987/COM-12-S(N)85