Benzene, 1-(2,2-dimethoxyethyl)-4-methoxy-

Base Information

Chemical Name:Benzene, 1-(2,2-dimethoxyethyl)-4-methoxy-
CAS No.:42866-92-2
Molecular Formula:C11H16 O3
Molecular Weight:196.246
Hs Code.:2911000000
Mol file:42866-92-2.mol

Synonyms:Acetaldehyde,(p-methoxyphenyl)-, dimethyl acetal (6CI,7CI); 4-(Methoxyphenyl)acetaldehydedimethyl acetal

Suppliers and Price of Benzene, 1-(2,2-dimethoxyethyl)-4-methoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
4-Methoxyphenylacetaldehyde dimethylacetal 95%
1g
$ 68.30

Crysdot
1-(2,2-Dimethoxyethyl)-4-methoxybenzene 95+%
10g
$ 319.00

Chemenu
1-(2,2-Dimethoxyethyl)-4-methoxybenzene 95%
10g
$ 301.00

American Custom Chemicals Corporation
4-METHOXYPHENYLACETALDEHYDE DIMETHYLACETAL 95.00%
1G
$ 673.08

Alichem
1-(2,2-Dimethoxyethyl)-4-methoxybenzene
10g
$ 400.00

AK Scientific
4-Methoxyphenylacetaldehyde dimethylacetal
1g
$ 136.00

Total 10 raw suppliers

Chemical Property of Benzene, 1-(2,2-dimethoxyethyl)-4-methoxy-

Chemical Property:

Refractive Index:n20/D1.504
Flash Point:>110℃
PSA：27.69000
Density:1.032 g/mL at 25 °C
LogP:1.85660

Purity/Quality:

97% ^*data from raw suppliers

4-Methoxyphenylacetaldehyde dimethylacetal 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Statements: 22-36/37/38
Safety Statements: 26

MSDS Files:

Useful:

Technology Process of Benzene, 1-(2,2-dimethoxyethyl)-4-methoxy-

There total 8 articles about Benzene, 1-(2,2-dimethoxyethyl)-4-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 67-56-1
methanol

: 637-69-4,24936-44-5
4-Methoxystyrene

: 42866-92-2
2-(4-methoxyphenyl)acetaldehyde dimethyl acetal

Guidance literature:: With Pyridine-2,6-dicarboxylic acid; iron(II) tetrafluoroborate hexahydrate; [bis(acetoxy)iodo]benzene; at 20 ℃; for 20h; regioselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1039/c2cc17889c

Reference yield:

: 5703-26-4
4-Methoxyphenylacetaldehyde

: 149-73-5
trimethyl orthoformate

: 42866-92-2
2-(4-methoxyphenyl)acetaldehyde dimethyl acetal

Guidance literature:: With magnesium sulfate; toluene-4-sulfonic acid; In methanol; dichloromethane; at -78 - 20 ℃;
DOI:10.1016/j.tet.2019.130883

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 42866-92-2
2-(4-methoxyphenyl)acetaldehyde dimethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 9.1 g / n-butyl-lithium / tetrahydrofuran; hexane / 1.) -78 --> -23 deg C, 1.5 h, 2.) 0 deg C, 14 h

2: 1.18 g / ceric ammonium nitrate / acetonitrile / 0.05 h / Ambient temperature

With n-butyllithium; ammonium cerium(IV) nitrate; In tetrahydrofuran; hexane; acetonitrile;