Technology Process of Benzene, 1-(2,2-dimethoxyethyl)-4-methoxy-
There total 8 articles about Benzene, 1-(2,2-dimethoxyethyl)-4-methoxy- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Pyridine-2,6-dicarboxylic acid; iron(II) tetrafluoroborate hexahydrate; [bis(acetoxy)iodo]benzene;
at 20 ℃;
for 20h;
regioselective reaction;
Molecular sieve;
Inert atmosphere;
DOI:10.1039/c2cc17889c
- Guidance literature:
-
With
magnesium sulfate; toluene-4-sulfonic acid;
In
methanol; dichloromethane;
at -78 - 20 ℃;
DOI:10.1016/j.tet.2019.130883
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 9.1 g / n-butyl-lithium / tetrahydrofuran; hexane / 1.) -78 --> -23 deg C, 1.5 h, 2.) 0 deg C, 14 h
2: 1.18 g / ceric ammonium nitrate / acetonitrile / 0.05 h / Ambient temperature
With
n-butyllithium; ammonium cerium(IV) nitrate;
In
tetrahydrofuran; hexane; acetonitrile;