C₁₅H₁₅BrFNO₂

Base Information

Chemical Name:C₁₅H₁₅BrFNO₂
CAS No.:1160359-90-9
Molecular Formula:C₁₅H₁₅BrFNO₂
Molecular Weight:340.192
Hs Code.:

C<sub>15</sub>H<sub>15</sub>BrFNO<sub>2</sub>

Synonyms:C₁₅H₁₅BrFNO₂

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Chemical Property of C₁₅H₁₅BrFNO₂

Chemical Property:

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Technology Process of C₁₅H₁₅BrFNO₂

There total 8 articles about C₁₅H₁₅BrFNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1128105-71-4
C₁₄H₁₁BrFNO₂

: 75-16-1
methylmagnesium bromide

: 1160359-90-9
C₁₅H₁₅BrFNO₂

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ml2000438

Reference yield:

: 1128105-71-4
C₁₄H₁₁BrFNO₂

: 676-58-4
methylmagnesium chloride

: 1160359-90-9
C₁₅H₁₅BrFNO₂

Guidance literature:: C₁₄H₁₁BrFNO₂; methylmagnesium chloride; With triethylamine; In tetrahydrofuran; at -78 ℃; for 4h;

With ammonium chloride; In tetrahydrofuran; ethyl acetate;

Reference yield:

: 1128105-86-1
C₁₅H₁₃BrFNO₃

: 1160359-90-9
C₁₅H₁₅BrFNO₂

Guidance literature:: Multi-step reaction with 5 steps

1: water; sodium hydroxide / methanol / 16 h / 20 °C / Inert atmosphere

2: pyridine; trifluoro-[1,3,5]triazine / dichloromethane / -10 - 20 °C / Inert atmosphere

3: sodium tetrahydroborate / methanol; dichloromethane / 2 h / 20 °C / Inert atmosphere

4: dipyridinium dichromate / dichloromethane / 4 h / 20 °C / Inert atmosphere

5: tetrahydrofuran; diethyl ether / 2 h / -78 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; dipyridinium dichromate; trifluoro-[1,3,5]triazine; water; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1021/ml2000438