(RS)-2-ethoxycarbonyl-2-(2-(ethoxycarbonyl)-5-methoxybenzyl)-6-methoxy-1-indanone

Base Information

Chemical Name:(RS)-2-ethoxycarbonyl-2-(2-(ethoxycarbonyl)-5-methoxybenzyl)-6-methoxy-1-indanone
CAS No.:867296-82-0
Molecular Formula:C₂₄H₂₆O₇
Molecular Weight:426.466
Hs Code.:

Synonyms:(RS)-2-ethoxycarbonyl-2-(2-(ethoxycarbonyl)-5-methoxybenzyl)-6-methoxy-1-indanone

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Chemical Property of (RS)-2-ethoxycarbonyl-2-(2-(ethoxycarbonyl)-5-methoxybenzyl)-6-methoxy-1-indanone

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Technology Process of (RS)-2-ethoxycarbonyl-2-(2-(ethoxycarbonyl)-5-methoxybenzyl)-6-methoxy-1-indanone

There total 2 articles about (RS)-2-ethoxycarbonyl-2-(2-(ethoxycarbonyl)-5-methoxybenzyl)-6-methoxy-1-indanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 56427-63-5
2-bromomethyl-4-methoxybenzoic acid ethyl ester

: 144067-29-8
ethyl 6-Methoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

: 867296-82-0
(RS)-2-ethoxycarbonyl-2-(2-(ethoxycarbonyl)-5-methoxybenzyl)-6-methoxy-1-indanone

Guidance literature:: ethyl 6-Methoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate; With sodium hydride; In N,N-dimethyl-formamide; at 60 ℃;

2-bromomethyl-4-methoxybenzoic acid ethyl ester; In N,N-dimethyl-formamide; at 60 ℃; for 44h;
DOI:10.1021/ja054322k

Reference yield:

: 56427-62-4
ethyl 4-methoxy-2-methylbenzoate

: 867296-82-0
(RS)-2-ethoxycarbonyl-2-(2-(ethoxycarbonyl)-5-methoxybenzyl)-6-methoxy-1-indanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-bromosuccinimide; dibenzoyl peroxide / CCl₄ / Heating

2.1: NaH / dimethylformamide / 60 °C

2.2: 85 percent / dimethylformamide / 44 h / 60 °C

With N-Bromosuccinimide; sodium hydride; dibenzoyl peroxide; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja054322k