Ethyl 4-methoxy-2-methylbenzoate

Base Information

• Chemical Name: Ethyl 4-methoxy-2-methylbenzoate
• CAS No.: 56427-62-4
• Molecular Formula: C11H14O3
• Molecular Weight: 194.23

Synonyms:ethyl 2-methyl-4-methoxybenzoate;4-Methoxy-2-methyl-benzoic acid ethyl ester;ethyl 4-methoxy-o-toluate;Benzoic acid, 4-methoxy-2-methyl-, ethyl ester;

Chemical Property of Ethyl 4-methoxy-2-methylbenzoate

Chemical Property:

• PSA: 35.53000
• LogP: 2.18030

Purity/Quality:

99% ^*data from raw suppliers

Ethyl4-Methoxy-2-methylbenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethyl 4-methoxy-2-methylbenzoate

There total 3 articles about Ethyl 4-methoxy-2-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

ethanol (64-17-5) + 4-methoxy-2-methylbenzoic acid (6245-57-4) → ethyl 4-methoxy-2-methylbenzoate (56427-62-4)

Guidance literature:

With thionyl chloride; for 4h; Reflux;

DOI:10.1016/j.bmcl.2008.05.019

Reference yield: 90.0%

methanol (67-56-1) + 4-carbethoxy-3-methyl-2-cyclohexen-1-one (487-51-4) → ethyl 4-methoxy-2-methylbenzoate (56427-62-4)

Guidance literature:

With iodine; for 0.5h; Heating;

DOI:10.1016/0040-4039(90)87013-P

Reference yield:

carbon monoxide (201230-82-2) + 4-bromo-3-methylanisole (27060-75-9) + O-ethyl di(tert-butyl)phosphinite (58309-95-8) → ethyl 4-methoxy-2-methylbenzoate (56427-62-4)

Guidance literature:

With palladium diacetate; at 115 ℃; for 18h; under 15001.5 Torr; Autoclave; Inert atmosphere;

DOI:10.1039/c7cc02828h

upstream raw materials:

methanol

4-carbethoxy-3-methyl-2-cyclohexen-1-one

ethanol

4-methoxy-2-methylbenzoic acid

Downstream raw materials:

(RS)-2-ethoxycarbonyl-2-(2-(ethoxycarbonyl)-5-methoxybenzyl)-6-methoxy-1-indanone

4-(2-carboxy-5-methoxybenzyloxy)phenylacetic acid

(RS)-2-ethoxycarbonyl-2-(2-(ethoxycarbonyl)-5-methoxybenzyl)-5-methoxy-1-indanone

2-bromomethyl-4-methoxybenzoic acid ethyl ester

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