7-(tert-butyldiphenylsilanyloxy)-6-(S)-methoxy heptanoic acid methyl ester

Base Information

Chemical Name:7-(tert-butyldiphenylsilanyloxy)-6-(S)-methoxy heptanoic acid methyl ester
CAS No.:1057663-74-7
Molecular Formula:C₂₃H₃₂O₂Si
Molecular Weight:368.591
Hs Code.:

Synonyms:7-(tert-butyldiphenylsilanyloxy)-6-(S)-methoxy heptanoic acid methyl ester

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Chemical Property of 7-(tert-butyldiphenylsilanyloxy)-6-(S)-methoxy heptanoic acid methyl ester

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Technology Process of 7-(tert-butyldiphenylsilanyloxy)-6-(S)-methoxy heptanoic acid methyl ester

There total 1 articles about 7-(tert-butyldiphenylsilanyloxy)-6-(S)-methoxy heptanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 313963-29-0
(S)-1-((tert-butyldiphenylsilyl)oxy)hex-5-en-2-ol

: 74-88-4
methyl iodide

: 1057663-74-7
7-(tert-butyldiphenylsilanyloxy)-6-(S)-methoxy heptanoic acid methyl ester

Guidance literature:: (S)-1-((tert-butyldiphenylsilyl)oxy)hex-5-en-2-ol; methyl iodide; With potassium hexamethylsilazane; In toluene; at -78 - 20 ℃; for 1.5h;

With water; ammonium chloride; In toluene;

Reference yield: 93.0%

: 1057663-74-7
7-(tert-butyldiphenylsilanyloxy)-6-(S)-methoxy heptanoic acid methyl ester

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: C₂₅H₃₄O₄Si

Guidance literature:: dichloro(tricyclohexylphosphino)(benzylidene)(1,3-dimesityl-4,5-dihydroimidazol-2-ylidene)ruthenium(III); In dichloromethane; at 20 ℃;

Reference yield:

: 1057663-74-7
7-(tert-butyldiphenylsilanyloxy)-6-(S)-methoxy heptanoic acid methyl ester

: 1057663-73-6
7-(tert-butyldiphenylsilanyloxy)-6-(S)-methoxy heptanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(tricyclohexylphosphino)(benzylidene)(1,3-dimesityl-4,5-dihydroimidazol-2-ylidene)ruthenium(III) / dichloromethane / 20 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 4 - 24 h

With hydrogen; dichloro(tricyclohexylphosphino)(benzylidene)(1,3-dimesityl-4,5-dihydroimidazol-2-ylidene)ruthenium(III); palladium 10% on activated carbon; In methanol; dichloromethane;