[4-{bis(2,4,6-triisopropylphenyl)phosphino}-3,5-diisopropylphenyl](3,5-di-tert-butyl-4-hydroxyphenyl)phenylmethanol

Base Information

Chemical Name:[4-{bis(2,4,6-triisopropylphenyl)phosphino}-3,5-diisopropylphenyl](3,5-di-tert-butyl-4-hydroxyphenyl)phenylmethanol
CAS No.:1335150-82-7
Molecular Formula:C₆₃H₈₉O₂P
Molecular Weight:909.372
Hs Code.:

Synonyms:[4-{bis(2,4,6-triisopropylphenyl)phosphino}-3,5-diisopropylphenyl](3,5-di-tert-butyl-4-hydroxyphenyl)phenylmethanol

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Chemical Property of [4-{bis(2,4,6-triisopropylphenyl)phosphino}-3,5-diisopropylphenyl](3,5-di-tert-butyl-4-hydroxyphenyl)phenylmethanol

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Technology Process of [4-{bis(2,4,6-triisopropylphenyl)phosphino}-3,5-diisopropylphenyl](3,5-di-tert-butyl-4-hydroxyphenyl)phenylmethanol

There total 3 articles about [4-{bis(2,4,6-triisopropylphenyl)phosphino}-3,5-diisopropylphenyl](3,5-di-tert-butyl-4-hydroxyphenyl)phenylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 40084-31-9
2,6-Di-tert-butyl-4-iodophenol

: 1335150-79-2
(4-benzoyl-2,6-diisopropylphenyl)bis(2,4,6-triisopropylphenyl)phosphine

: 1335150-82-7
[4-{bis(2,4,6-triisopropylphenyl)phosphino}-3,5-diisopropylphenyl](3,5-di-tert-butyl-4-hydroxyphenyl)phenylmethanol

Guidance literature:: 2,6-Di-tert-butyl-4-iodophenol; With n-butyllithium; In diethyl ether; hexane; at -78 - 20 ℃; Inert atmosphere;

(4-benzoyl-2,6-diisopropylphenyl)bis(2,4,6-triisopropylphenyl)phosphine; In diethyl ether; hexane; at -78 - 20 ℃; Inert atmosphere;

With water; ammonium chloride; In diethyl ether; hexane; Inert atmosphere;
DOI:10.1016/j.jorganchem.2011.07.013

Reference yield:

: 958007-24-4
(4-bromo-2,6-diisopropylphenyl)bis(2,4,6-triisopropylphenyl)phosphine

: 1335150-82-7
[4-{bis(2,4,6-triisopropylphenyl)phosphino}-3,5-diisopropylphenyl](3,5-di-tert-butyl-4-hydroxyphenyl)phenylmethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

1.3: Inert atmosphere

2.1: n-butyllithium / diethyl ether; hexane / -78 - 20 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

2.3: Inert atmosphere

With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1016/j.jorganchem.2011.07.013

Reference yield:

: 100-47-0
benzonitrile

: 1335150-82-7
[4-{bis(2,4,6-triisopropylphenyl)phosphino}-3,5-diisopropylphenyl](3,5-di-tert-butyl-4-hydroxyphenyl)phenylmethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

1.3: Inert atmosphere

2.1: n-butyllithium / diethyl ether; hexane / -78 - 20 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

2.3: Inert atmosphere

With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1016/j.jorganchem.2011.07.013