3'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityI)-2'-deoxy-5-methylthiouridine

Base Information

Chemical Name:3'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityI)-2'-deoxy-5-methylthiouridine
CAS No.:1256466-55-3
Molecular Formula:C₃₇H₄₆N₂O₇SSi
Molecular Weight:690.933
Hs Code.:

Synonyms:3'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityI)-2'-deoxy-5-methylthiouridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityI)-2'-deoxy-5-methylthiouridine

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Technology Process of 3'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityI)-2'-deoxy-5-methylthiouridine

There total 1 articles about 3'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityI)-2'-deoxy-5-methylthiouridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 624-92-0
Dimethyldisulphide

: 364613-26-3
3'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxy-5-iodouridine

: 1256466-55-3
3'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityI)-2'-deoxy-5-methylthiouridine

Guidance literature:: 3'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxy-5-iodouridine; With hydrogen; sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

Dimethyldisulphide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1.75h;