3-(Aminomethyl)cyclohexylamine

Base Information

• Chemical Name: 3-(Aminomethyl)cyclohexylamine
• CAS No.: 97087-59-7
• Molecular Formula: C7H16 N2
• Molecular Weight: 128.21
• Hs Code.: 2921300090
• Mol file: 97087-59-7.mol

Synonyms:3-(Aminomethyl)cyclohexylamine;3-Aminomethyl-1-cyclohexylamine; a-(3-Aminocyclohexyl)methylamine

Chemical Property of 3-(Aminomethyl)cyclohexylamine

Chemical Property:

• Vapor Pressure: 0.298mmHg at 25°C
• Boiling Point: 202.062°C at 760 mmHg
• Flash Point: 87.54°C
• PSA: 52.04000
• Density: 0.924g/cm³
• LogP: 1.86320

Purity/Quality:

99% ^*data from raw suppliers

3-(Aminomethyl)cyclohexylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(Aminomethyl)cyclohexylamine

There total 2 articles about 3-(Aminomethyl)cyclohexylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

m-aminobenzylamine (4403-70-7) → α-(3-aminocyclohexyl)methylamine (97087-59-7,1206798-46-0,1206798-47-1)

Guidance literature:

Reference yield:

4-cyanocyclohexanone (34916-10-4) + (RS)-3-oxocyclohexanecarbonitrile (17983-30-1) → α-(3-aminocyclohexyl)methylamine (97087-59-7,1206798-46-0,1206798-47-1) + 1-amino-4-(aminomethyl)cyclohexane (13338-82-4)

Guidance literature:

4-cyanocyclohexanone; (RS)-3-oxocyclohexanecarbonitrile; With ammonia; at 80 ℃; for 2h; under 37503.8 Torr; Inert atmosphere; Autoclave;

With hydrogen; Raney cobalt; at 120 ℃; for 3h; under 112511 - 150015 Torr; Product distribution / selectivity; Inert atmosphere; Autoclave;

Reference yield:

phosgene (75-44-5) + α-(3-aminocyclohexyl)methylamine (97087-59-7,1206798-46-0,1206798-47-1) → α-(3-isocyanatocyclohexyl)methylisocyanate (133078-88-3)

Guidance literature:

With hydrogenchloride; In 1-pentyl acetate;

upstream raw materials:

m-aminobenzylamine

4-cyanocyclohexanone

(RS)-3-oxocyclohexanecarbonitrile

Downstream raw materials:

α-(3-isocyanatocyclohexyl)methylisocyanate

Refernces

• 1、 -. "Alicyclic diamines, alicyclic diisocyanates and polyisocyanato-isocyanurates and method for the preparation thereof". . . Retrieved 2008/06/13.