N-[(4-methoxyphenyl)methylidene]-2,3-dibromopropylamine

Base Information

• Chemical Name: N-[(4-methoxyphenyl)methylidene]-2,3-dibromopropylamine
• CAS No.: 160676-78-8
• Molecular Formula: C₁₁H₁₃Br₂NO
• Molecular Weight: 335.038
• Mol file: 160676-78-8.mol

Synonyms:N-[(4-methoxyphenyl)methylidene]-2,3-dibromopropylamine

Chemical Property of N-[(4-methoxyphenyl)methylidene]-2,3-dibromopropylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[(4-methoxyphenyl)methylidene]-2,3-dibromopropylamine

There total 3 articles about N-[(4-methoxyphenyl)methylidene]-2,3-dibromopropylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-[(E)-(4-methoxyphenyl)methylidene]prop-2-en-1-amine (27976-88-1) → N-[(4-methoxyphenyl)methylidene]-2,3-dibromopropylamine (160676-78-8)

Guidance literature:

With bromine; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1021/jo048486f

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → N-[(4-methoxyphenyl)methylidene]-2,3-dibromopropylamine (160676-78-8)

Guidance literature:

Multi-step reaction with 2 steps

1: magnesium sulfate / CH₂Cl₂ / 1 h / Heating

2: 100 percent / bromine / CH₂Cl₂ / 0.5 h / 20 °C

With bromine; magnesium sulfate; In dichloromethane;

DOI:10.1021/jo048486f

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → N-[(4-methoxyphenyl)methylidene]-2,3-dibromopropylamine (160676-78-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 93 percent / MgSO₄*3H₂O / CH₂Cl₂ / 1 h / 20 °C

2: Br₂ / CH₂Cl₂ / 0.5 h / 0 °C

With bromine; magnesium sulfate; In dichloromethane;

DOI:10.1016/S0040-4020(02)00728-7

upstream raw materials:

N-[(E)-(4-methoxyphenyl)methylidene]prop-2-en-1-amine

4-methoxy-benzaldehyde

Downstream raw materials:

N-allyl-4-methoxybenzylamine

1-(4-methoxyphenyl)methyl-2-(thiocyanatomethyl)aziridine

2-bromomethyl-1-[(4-methoxyphenyl)methyl]aziridine