[(4-Methoxyphenyl)methyl](prop-2-en-1-yl)amine

Base Information

• Chemical Name: [(4-Methoxyphenyl)methyl](prop-2-en-1-yl)amine
• CAS No.: 86926-56-9
• Molecular Formula: C₁₁H₁₅NO
• Molecular Weight: 177.246
• European Community (EC) Number: 823-517-0
• Nikkaji Number: J896.530G
• Mol file: 86926-56-9.mol

Synonyms:[(4-methoxyphenyl)methyl](prop-2-en-1-yl)amine;86926-56-9;N-[(4-methoxyphenyl)methyl]prop-2-en-1-amine;N-(4-methoxybenzyl)prop-2-en-1-amine;4-Methoxybenzylallylamine;N-allyl-4-methoxybenzylamine;SCHEMBL5577604;N-allyl-N-(4-methoxybenzyl)amine;MFCD07406339;AKOS000224215;EN300-50975

Chemical Property of [(4-Methoxyphenyl)methyl](prop-2-en-1-yl)amine

Chemical Property:

• Boiling Point: 265.5±20.0 °C(Predicted)
• PKA: 9.29±0.20(Predicted)
• Density: 0.967±0.06 g/cm3(Predicted)
• XLogP3: 2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 177.115364102
• Heavy Atom Count: 13
• Complexity: 139

Purity/Quality:

99% ^*data from raw suppliers

[(4-methoxyphenyl)methyl](prop-2-en-1-yl)amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)CNCC=C

Technology Process of [(4-Methoxyphenyl)methyl](prop-2-en-1-yl)amine

There total 18 articles about [(4-Methoxyphenyl)methyl](prop-2-en-1-yl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

p-methoxybenzyl chloride (824-94-2) + 1-amino-2-propene (107-11-9,30551-89-4) → N-allyl-4-methoxybenzylamine (86926-56-9)

Guidance literature:

With potassium carbonate; In neat (no solvent); at 20 ℃;

Reference yield: 97.0%

4-methoxy-benzaldehyde (123-11-5) + 1-amino-2-propene (107-11-9,30551-89-4) → N-allyl-4-methoxybenzylamine (86926-56-9)

Guidance literature:

4-methoxy-benzaldehyde; 1-amino-2-propene; In methanol; at 0 ℃; for 1h;

With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.5h;

DOI:10.1055/s-0034-1379985

Reference yield: 94.0%

N-Allyl-N-(4-methoxy-benzyl)-2,4-dinitro-benzenesulfonamide (196214-38-7) → N-allyl-4-methoxybenzylamine (86926-56-9)

Guidance literature:

With mercaptoacetic acid; triethylamine; In dichloromethane; at 23 ℃; for 0.0833333h;

DOI:10.1016/S0040-4039(97)01334-8

upstream raw materials:

N-Allyl-N-(4-methoxy-benzyl)-2,4-dinitro-benzenesulfonamide

1-amino-2-propene

4-Methoxybenzyl alcohol

2-bromomethyl-1-[(4-methoxyphenyl)methyl]aziridine

Downstream raw materials:

{[Allyl-(4-methoxy-benzyl)-carbamoyl]-methyl}-(2-bromo-benzyl)-carbamic acid tert-butyl ester

N-allyl-N-propargyl-4-methoxybenzylamine

(1S)-N-allyl-N-(4-methoxy-benzyl)-1-phenyl-allylamine

(R)-4-{(R)-[Allyl-(4-methoxy-benzyl)-amino]-phenyl-methyl}-[1,3]dioxolane-2-thione