3-HYDROXYBENZOIC ACID SODIUM SALT

Base Information

• Chemical Name: 3-HYDROXYBENZOIC ACID SODIUM SALT
• CAS No.: 7720-19-6
• Molecular Formula: C7H5NaO3
• Molecular Weight: 160.105
• Hs Code.: 2918290000
• Mol file: 7720-19-6.mol

Synonyms:Benzoicacid, 3-hydroxy-, monosodium salt (9CI);Benzoic acid, m-hydroxy-, monosodiumsalt (8CI);Monosodium 3-hydroxybenzoate;Monosodium m-hydroxybenzoate;Sodium3-hydroxybenzoate;Sodium m-hydroxybenzoate;Sodium m-hydroxybenzoate;m-Hydroxybenzoic acid monosodium salt;

Chemical Property of 3-HYDROXYBENZOIC ACID SODIUM SALT

Chemical Property:

• Vapor Pressure: 2.24E-05mmHg at 25°C
• Boiling Point: 346.1 °C at 760 mmHg
• Flash Point: 177.3 °C
• PSA: 60.36000
• LogP: -0.24430
• Storage Temp.: Inert atmosphere,Room Temperature
• Water Solubility.: almost transparency

Purity/Quality:

99% ^*data from raw suppliers

Sodium 3-Hydroxybenzoate >99.0%(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-HYDROXYBENZOIC ACID SODIUM SALT

There total 1 articles about 3-HYDROXYBENZOIC ACID SODIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium benzoate (532-32-1) → m-hydroxybenzoic acid sodium salt (7720-19-6) + sodium salicylate (54-21-7) + sodium 4-hydroxybenzoate (114-63-6)

Guidance literature:

With phosphate buffer; Saline; 2-Deoxy-D-ribose; dinitrogen monoxide; at 20 - 25 ℃; for 1h; Irradiation; var. OH scavengers;

DOI:10.1248/cpb.41.1842

Reference yield: 77.0%

sodium benzoate (532-32-1) + vanadyl(IV) sulfate hydrate + m-hydroxybenzoic acid sodium salt (7720-19-6) → oxovanadium(IV) (benzoate)(3-hydroxybenzoate) (130565-58-1)

Guidance literature:

In methanol; water; sodium hydroxybenzoate in water mixed with sodium benzoate in water, warmed (hot plate), dropwise addn. of VO(SO4) in 50% MeOH/H2O soln. with stirring, complex pptd. immediately; filtered, washed (hot 50% MeOH/H2O), dried (vac., anhyd. silica gel); elem. anal.;

Reference yield: 58.0%

vanadium(IV) chloride + m-hydroxybenzoic acid sodium salt (7720-19-6) → oxovanadium(IV) monochloro(3-hydroxybenzoate) (130565-55-8) + oxovanadium(IV) monochloro(3-hydroxybenzoate)*H2O (130565-54-7)

Guidance literature:

In methanol; water; sodium salt and VOCl2 refluxed in MeOH/H2O (1:1) with stirring, rapid pptn. complex; filtered, washed (hot 50% MeOH/H2O), dried (vac., anhyd. silica gel); complex VOCl(3-HOC6H4COO) from filtrate left overnight (pptn.); elem. anal.;

upstream raw materials:

sodium benzoate

Downstream raw materials:

oxovanadium(IV) (benzoate)(3-hydroxybenzoate)

oxovanadium(IV) monochloro(3-hydroxybenzoate)

oxovanadium(IV) monochloro(3-hydroxybenzoate)*H₂O

trans-diaquabis(3-hydroxybenzoato-O)bis(nicotinamide-N⁽¹⁾)cobalt(II)

Refernces