(R,E)-ethyl-2-(2-(tert-butyldimethylsilyloxy)ethyl)-6-(4-methoxybenzyloxy)-5-(triisopropylsilyloxy)hex-2-enoate

Base Information

Chemical Name:(R,E)-ethyl-2-(2-(tert-butyldimethylsilyloxy)ethyl)-6-(4-methoxybenzyloxy)-5-(triisopropylsilyloxy)hex-2-enoate
CAS No.:1164114-90-2
Molecular Formula:C₃₃H₆₀O₆Si₂
Molecular Weight:609.007
Hs Code.:

Synonyms:(R,E)-ethyl-2-(2-(tert-butyldimethylsilyloxy)ethyl)-6-(4-methoxybenzyloxy)-5-(triisopropylsilyloxy)hex-2-enoate

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Chemical Property of (R,E)-ethyl-2-(2-(tert-butyldimethylsilyloxy)ethyl)-6-(4-methoxybenzyloxy)-5-(triisopropylsilyloxy)hex-2-enoate

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Technology Process of (R,E)-ethyl-2-(2-(tert-butyldimethylsilyloxy)ethyl)-6-(4-methoxybenzyloxy)-5-(triisopropylsilyloxy)hex-2-enoate

There total 2 articles about (R,E)-ethyl-2-(2-(tert-butyldimethylsilyloxy)ethyl)-6-(4-methoxybenzyloxy)-5-(triisopropylsilyloxy)hex-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1164115-08-5
C₃₁H₅₆O₆Si₂

: 75-03-6
ethyl iodide

: 1164114-90-2
(R,E)-ethyl-2-(2-(tert-butyldimethylsilyloxy)ethyl)-6-(4-methoxybenzyloxy)-5-(triisopropylsilyloxy)hex-2-enoate

Guidance literature:: With potassium carbonate; In water; acetone; at 20 ℃; for 15h;
DOI:10.1021/ol900757k

Reference yield: 93.0%

: C₃₇H₇₀O₆Si₃

: 75-03-6
ethyl iodide

: 1164114-90-2
(R,E)-ethyl-2-(2-(tert-butyldimethylsilyloxy)ethyl)-6-(4-methoxybenzyloxy)-5-(triisopropylsilyloxy)hex-2-enoate

Guidance literature:: With potassium carbonate; In water; acetone; at 20 ℃; for 15h;
DOI:10.1002/chem.201000104

Reference yield:

: 1164114-90-2
(R,E)-ethyl-2-(2-(tert-butyldimethylsilyloxy)ethyl)-6-(4-methoxybenzyloxy)-5-(triisopropylsilyloxy)hex-2-enoate

: C₃₃H₆₂O₈Si₂

: 1164115-09-6
C₃₃H₆₂O₈Si₂

Guidance literature:: With potassium osmate; hydroquinindine-2,5-diphenyl-4,6-pyrimidinediyl diether; methanesulfonamide; water; potassium carbonate; potassium hexacyanoferrate(III); In tert-butyl alcohol; at 0 ℃; for 72h; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/ol900757k