(p-ethoxycarbonylphenyl)ferrocene

Base Information

Chemical Name:(p-ethoxycarbonylphenyl)ferrocene
CAS No.:58482-66-9
Molecular Formula:C₁₉H₁₈FeO₂
Molecular Weight:334.198
Hs Code.:

Synonyms:(p-ethoxycarbonylphenyl)ferrocene

Suppliers and Price of (p-ethoxycarbonylphenyl)ferrocene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (p-ethoxycarbonylphenyl)ferrocene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (p-ethoxycarbonylphenyl)ferrocene

There total 4 articles about (p-ethoxycarbonylphenyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1274-09-5
bis(ferrocenyl)mercury

: 51934-41-9
4-iodobenzoic acid ethyl ester

: 58482-66-9
(p-ethoxycarbonylphenyl)ferrocene

Guidance literature:: With NaI; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; acetone; Fe-complex, ligand and NaI in THF and acetone were placed under Ar, mixt. heated to boiling, Pd-complex was added, refluxed for 1.5 h; filtered, evapd. in vac., column chromy. with benzene-hexane;
DOI:10.1016/S0022-328X(01)00979-2

Reference yield: 53.0%

: para-(ferrocenyl)benzoic acid

: 64-17-5
ethanol

: 58482-66-9
(p-ethoxycarbonylphenyl)ferrocene

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2016.07.027

Reference yield: 26.0%

: 102-54-5,55404-68-7
ferrocene

: 4-Ethoxycarbonyl-benzenediazonium; hydrogen sulfate

: 58482-66-9
(p-ethoxycarbonylphenyl)ferrocene

: 87607-45-2
1,1'-bis[p-(ethoxycarbonyl)phenyl]ferrocene

Guidance literature:: In water; acetic acid; soln. of diazotized salt in 10% sulfuric acid added rapidly to soln. offerrocene in acetic acid under N2, stirred overnight at room temp., poured into water; extd. with CHCl3, ext. washed with 5% aq. NaHCO3 and brine, dried over anhyd. MgSO4, filtered, concd., purified by column chromy. (SiO2, benzene); elem. anal.;
DOI:10.1246/bcsj.56.2023