diphenoxyacetyl chloride

Base Information Edit

Chemical Name:diphenoxyacetyl chloride
CAS No.:39628-29-0
Molecular Formula:C₁₄H₁₁ClO₃
Molecular Weight:262.693
Hs Code.:
Mol file:39628-29-0.mol

Synonyms:diphenoxyacetyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenoxyacetyl chloride Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of diphenoxyacetyl chloride

There total 1 articles about diphenoxyacetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 729-89-5
1,1-bisacetic acid

: 39628-29-0
diphenoxyacetyl chloride

Guidance literature:: With pyridine; thionyl chloride; diethyl ether;

Reference yield: 38.0%

: 13859-41-1
sodium-manganese pentacarbonyl

: 39628-29-0
diphenoxyacetyl chloride

: ((C₆H₅)O)2CHCOMn(CO)5

: 7647-14-5
sodium chloride

Guidance literature:: In tetrahydrofuran; under N2; soln. of 5mmol NaMn(CO)5 in THF cooled to -78°C, 5.25 mmol (PhO)2CHCOCl added; mixt. warmed up to room temp., then stirred overnight; pptd. NaCl filtered off, solvent removed; residue extd. with petroleum ether; chromy. (silica gel, petroleum ether/ether (10:1));pentane soln. cooled, recrystn. from petroleum ether at -80°C; elem anal.;