cyclodecasulfur

Base Information Edit

Chemical Name:cyclodecasulfur
CAS No.:106763-15-9
Molecular Formula:S₁₀
Molecular Weight:320.66
Hs Code.:
Mol file:106763-15-9.mol

Synonyms:cyclodecasulfur

Suppliers and Price of cyclodecasulfur

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclodecasulfur Edit

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of cyclodecasulfur

There total 7 articles about cyclodecasulfur which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 7791-25-5
sulfuryl dichloride

: bis(η-cyclopentadienyl)titana(IV)cyclohexasulfane

: 1271-19-8
bis(cyclopentadienyl)titanium dichloride

: 106763-15-9
cyclodecasulfur

: 42817-30-1
S₂₀

Guidance literature:: In carbon disulfide; byproducts: S7, S8, S9; complex and CS2 stirred for 10 min at 25°C with exclusion of moisture, SO2Cl2 soln. rapidly added with stirring, reacted for 30 min; further by-products: S12, S14, S15, S16, S19, S25, S30; filtered, concd. at 70°C, dried over MgSO4, cooled to -78°C, pptd. for 7-10 d, rapidly filtered, extd. (CS2 at 25°C for 15min) with crushing, crude product washed with CS2, then with CHCl3, dried in air, recrystd. (CS2);

Reference yield:

: 13798-23-7
hexasulfur

: 10544-50-0
sulfur

: 106763-15-9
cyclodecasulfur

: 14999-38-3
cyclo-dodecasulfur

: 21459-04-1
sulfur

Guidance literature:: In carbon disulfide; byproducts: S9, S11, S14; Irradiation (UV/VIS); photolysis (high pressure Hg lamp, 200-600 nm), 15°C; further product: S5 (traces); monitoring by HPL chromy.; Kinetics;