(+)-(S)-1-(1,2-diphenyl-ethylideneamino)-2-methoxymethyl pyrrolidine

Base Information Edit

Chemical Name:(+)-(S)-1-(1,2-diphenyl-ethylideneamino)-2-methoxymethyl pyrrolidine
CAS No.:107538-62-5
Molecular Formula:C₂₀H₂₄N₂O
Molecular Weight:308.423
Hs Code.:
Mol file:107538-62-5.mol

Synonyms:(+)-(S)-1-(1,2-diphenyl-ethylideneamino)-2-methoxymethyl pyrrolidine

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Chemical Property of (+)-(S)-1-(1,2-diphenyl-ethylideneamino)-2-methoxymethyl pyrrolidine Edit

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Technology Process of (+)-(S)-1-(1,2-diphenyl-ethylideneamino)-2-methoxymethyl pyrrolidine

There total 5 articles about (+)-(S)-1-(1,2-diphenyl-ethylideneamino)-2-methoxymethyl pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 451-40-1
phenyl benzyl ketone

: 59983-39-0,187035-29-6
(S)-1-amino-2-(methoxymethyl)pyrrolidine

: 107538-62-5
(+)-(S)-1-(1,2-diphenyl-ethylideneamino)-2-methoxymethyl pyrrolidine

Guidance literature:: In benzene; for 24h; Heating;
DOI:10.1016/S0040-4020(01)82420-0

Reference yield:

: 60096-50-6
(S)-N-Nitroso-O-methylprolinol

: 107538-62-5
(+)-(S)-1-(1,2-diphenyl-ethylideneamino)-2-methoxymethyl pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran

With lithium aluminium tetrahydride; In tetrahydrofuran;

Reference yield:

: 89999-42-8
(S)-2-methoxymethyl-1-(3-phenylpropylidenamino)pyrrolidine

: 107538-62-5
(+)-(S)-1-(1,2-diphenyl-ethylideneamino)-2-methoxymethyl pyrrolidine

Guidance literature:: Multi-step reaction with 4 steps

1: 1) lithium diisopropylamide / 1) ether, 0 deg C, 4 h, 2) -78 deg C, 2 h; 10 h, -78 deg C to RT

2: O₃ / pentane / -78 °C

3: LiAlH₄ / tetrahydrofuran

With lithium aluminium tetrahydride; ozone; lithium diisopropyl amide; In tetrahydrofuran; pentane;