10-methoxy-8-(4-methylphenyl)-13H-benzo[f]indolo[3,2-c]quinoline

Base Information

• Chemical Name: 10-methoxy-8-(4-methylphenyl)-13H-benzo[f]indolo[3,2-c]quinoline
• CAS No.: 1429117-75-8
• Molecular Formula: C₂₇H₂₀N₂O
• Molecular Weight: 388.469
• Mol file: 1429117-75-8.mol

Synonyms:10-methoxy-8-(4-methylphenyl)-13H-benzo[f]indolo[3,2-c]quinoline

Chemical Property of 10-methoxy-8-(4-methylphenyl)-13H-benzo[f]indolo[3,2-c]quinoline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 10-methoxy-8-(4-methylphenyl)-13H-benzo[f]indolo[3,2-c]quinoline

There total 6 articles about 10-methoxy-8-(4-methylphenyl)-13H-benzo[f]indolo[3,2-c]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

5-methoxylindole (1006-94-6) + 2-(4-methylbenzylideneamino)naphthalene (53501-68-1) → 10-methoxy-8-(4-methylphenyl)-13H-benzo[f]indolo[3,2-c]quinoline (1429117-75-8)

Guidance literature:

5-methoxylindole; 2-(4-methylbenzylideneamino)naphthalene; With iodine; In N,N-dimethyl acetamide; at 80 ℃; for 16h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In N,N-dimethyl acetamide; at 80 ℃;

DOI:10.1002/cjoc.201200993

Reference yield:

5-methoxylindole (1006-94-6) + 2-(4-methylbenzylideneamino)naphthalene (53501-68-1) → 10-methoxy-8-(4-methylphenyl)-13H-benzo[f]indolo[3,2-c]quinoline (1429117-75-8) + C27H22N2O

Guidance literature:

With iodine; In N,N-dimethyl acetamide; at 80 ℃; for 16h;

DOI:10.1002/cjoc.201200993

Reference yield:

naphthalen-2-ylamine (91-59-8) → 10-methoxy-8-(4-methylphenyl)-13H-benzo[f]indolo[3,2-c]quinoline (1429117-75-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: benzene / Reflux

2.1: iodine / N,N-dimethyl acetamide / 16 h / 80 °C

2.2: 80 °C

With iodine; In N,N-dimethyl acetamide; benzene;

DOI:10.1002/cjoc.201200993

upstream raw materials:

5-methoxylindole

2-(4-methylbenzylideneamino)naphthalene

naphthalen-2-ylamine

4-methyl-benzaldehyde