C₃₀H₃₃Cl₂FN₄O₇

Base Information

Chemical Name:C₃₀H₃₃Cl₂FN₄O₇
CAS No.:1201916-81-5
Molecular Formula:C₃₀H₃₃Cl₂FN₄O₇
Molecular Weight:651.519
Hs Code.:

C<sub>30</sub>H<sub>33</sub>Cl<sub>2</sub>FN<sub>4</sub>O<sub>7</sub>

Synonyms:C₃₀H₃₃Cl₂FN₄O₇

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Chemical Property of C₃₀H₃₃Cl₂FN₄O₇

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Technology Process of C₃₀H₃₃Cl₂FN₄O₇

There total 6 articles about C₃₀H₃₃Cl₂FN₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1040377-28-3
5-[(2,6-dichloro-3-fluorophenyl)ethoxy]-6-{(ert-butoxy)-N-[(tert-butyl)oxycarbonyl]carbonylamino}pyridazine-3-carboxylic acid

: 104-94-9
4-methoxy-aniline

: 1201916-81-5
C₃₀H₃₃Cl₂FN₄O₇

Guidance literature:: 5-[(2,6-dichloro-3-fluorophenyl)ethoxy]-6-{(ert-butoxy)-N-[(tert-butyl)oxycarbonyl]carbonylamino}pyridazine-3-carboxylic acid; With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

4-methoxy-aniline; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

Reference yield:

: 756520-66-8
1-(2,6-dichloro-3-fluorophenyl)ethanol

: 1201916-81-5
C₃₀H₃₃Cl₂FN₄O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

1.2: Reflux

2.1: dmap / N,N-dimethyl-formamide / 20 °C

3.1: sodium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / N,N-dimethyl-formamide / 1.5 h / 90 °C

4.1: water; lithium hydroxide / tetrahydrofuran / 20 °C

4.2: pH 5

5.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 20 °C

5.2: 0.5 h / 20 °C

With dmap; water; sodium acetate; sodium hydride; N-ethyl-N,N-diisopropylamine; HATU; lithium hydroxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 1040376-43-9
6-chloro-4-[1-(2,6-dichloro-3-fluoro-phenyl)-ethoxy]-pyridazin-3-ylamine

: 1201916-81-5
C₃₀H₃₃Cl₂FN₄O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap / N,N-dimethyl-formamide / 20 °C

2.1: sodium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / N,N-dimethyl-formamide / 1.5 h / 90 °C

3.1: water; lithium hydroxide / tetrahydrofuran / 20 °C

3.2: pH 5

4.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.2: 0.5 h / 20 °C

With dmap; water; sodium acetate; N-ethyl-N,N-diisopropylamine; HATU; lithium hydroxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; N,N-dimethyl-formamide;