2-Acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

Base Information

Chemical Name:2-Acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid
CAS No.:136408-91-8
Molecular Formula:C₁₈H₂₅NO₇
Molecular Weight:367.399
Hs Code.:

Synonyms:2-Acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

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Chemical Property of 2-Acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

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Technology Process of 2-Acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

There total 9 articles about 2-Acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54400-75-8
allyl 2-acetamido-2-deoxy-α-D-glucopyranoside

: 136408-91-8
2-Acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

Guidance literature:: Multi-step reaction with 7 steps

1: 91 percent / CSA / acetonitrile / 0.5 h

2: 93 percent / pyridine / 12 h

3: 50 percent / NaBH₃CN, molecular sieve 3 Angstroem, trifluoroacetic acid / tetrahydrofuran / 16 h / 0 °C

4: 65 percent / pyridine / CH₂Cl₂ / 2 h / Ambient temperature

5: 69 percent / LiCl, HMPT / 3 h / Heating

6: 53 percent / Bu₃SnH, AIBN / toluene / 110 °C

7: 93 percent / AcOH / Pd(OAc)2 / H₂O / a) 1 d, room temp., b) 1 h, 40 deg C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; 2,2'-azobis(isobutyronitrile); 3 A molecular sieve; camphor-10-sulfonic acid; tri-n-butyl-tin hydride; sodium cyanoborohydride; acetic acid; trifluoroacetic acid; lithium chloride; palladium diacetate; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 136408-91-8
2-Acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

Guidance literature:: Multi-step reaction with 7 steps

1: 91 percent / CSA / acetonitrile / 0.5 h

2: 93 percent / pyridine / 12 h

3: 50 percent / NaBH₃CN, molecular sieve 3 Angstroem, trifluoroacetic acid / tetrahydrofuran / 16 h / 0 °C

4: 65 percent / pyridine / CH₂Cl₂ / 2 h / Ambient temperature

5: 69 percent / LiCl, HMPT / 3 h / Heating

6: 53 percent / Bu₃SnH, AIBN / toluene / 110 °C

7: 93 percent / AcOH / Pd(OAc)2 / H₂O / a) 1 d, room temp., b) 1 h, 40 deg C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; 2,2'-azobis(isobutyronitrile); 3 A molecular sieve; camphor-10-sulfonic acid; tri-n-butyl-tin hydride; sodium cyanoborohydride; acetic acid; trifluoroacetic acid; lithium chloride; palladium diacetate; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 136408-91-8
2-Acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

Guidance literature:: Multi-step reaction with 7 steps

1: 80 percent / HC(OCH₃)3, CSA / dimethylformamide / 6 h

2: 93 percent / pyridine / 12 h

3: 50 percent / NaBH₃CN, molecular sieve 3 Angstroem, trifluoroacetic acid / tetrahydrofuran / 16 h / 0 °C

4: 65 percent / pyridine / CH₂Cl₂ / 2 h / Ambient temperature

5: 69 percent / LiCl, HMPT / 3 h / Heating

6: 53 percent / Bu₃SnH, AIBN / toluene / 110 °C

7: 93 percent / AcOH / Pd(OAc)2 / H₂O / a) 1 d, room temp., b) 1 h, 40 deg C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; 2,2'-azobis(isobutyronitrile); 3 A molecular sieve; camphor-10-sulfonic acid; tri-n-butyl-tin hydride; sodium cyanoborohydride; acetic acid; trifluoroacetic acid; lithium chloride; trimethyl orthoformate; palladium diacetate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;