Technology Process of C10H15BO5
There total 4 articles about C10H15BO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
n-butyllithium; Triisopropyl borate;
In
tetrahydrofuran; hexanes;
at -78 - 20 ℃;
Cooling with acetone-dry ice;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: bromine; sodium acetate; acetic acid / 20 °C
2.1: water; potassium hydroxide / methanol / 0.5 h / 20 °C
2.2: Acidic aqueous solution
3.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 100 °C
4.1: n-butyllithium; Triisopropyl borate / tetrahydrofuran; hexanes / -78 - 20 °C / Cooling with acetone-dry ice; Inert atmosphere
With
n-butyllithium; Triisopropyl borate; water; bromine; sodium acetate; potassium carbonate; acetic acid; potassium hydroxide;
In
tetrahydrofuran; methanol; hexanes; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 100 °C
2: n-butyllithium; Triisopropyl borate / tetrahydrofuran; hexanes / -78 - 20 °C / Cooling with acetone-dry ice; Inert atmosphere
With
n-butyllithium; Triisopropyl borate; potassium carbonate;
In
tetrahydrofuran; hexanes; N,N-dimethyl-formamide;