Technology Process of C26H33N5O2Si
There total 4 articles about C26H33N5O2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
caesium carbonate;
tris-(dibenzylideneacetone)dipalladium(0); XPhos;
In
tert-butyl alcohol;
at 100 ℃;
for 3h;
microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen / Raney nickel / tetrahydrofuran; methanol / 2250.23 Torr
2: caesium carbonate / tris-(dibenzylideneacetone)dipalladium(0); XPhos / tert-butyl alcohol / 3 h / 100 °C / microwave irradiation
With
hydrogen; caesium carbonate;
tris-(dibenzylideneacetone)dipalladium(0); XPhos;
In
tetrahydrofuran; methanol; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 7 h / 100 °C / Inert atmosphere
2: hydrogen / Raney nickel / tetrahydrofuran; methanol / 2250.23 Torr
3: caesium carbonate / tris-(dibenzylideneacetone)dipalladium(0); XPhos / tert-butyl alcohol / 3 h / 100 °C / microwave irradiation
With
hydrogen; sodium carbonate; caesium carbonate;
tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0); XPhos;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; tert-butyl alcohol;