4,4-Dimethylpent-2-enanilid

Base Information

Chemical Name:4,4-Dimethylpent-2-enanilid
CAS No.:17767-01-0
Molecular Formula:C₁₃H₁₇NO
Molecular Weight:203.284
Hs Code.:

Synonyms:4,4-Dimethylpent-2-enanilid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4-Dimethylpent-2-enanilid

Chemical Property:

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Technology Process of 4,4-Dimethylpent-2-enanilid

There total 5 articles about 4,4-Dimethylpent-2-enanilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 61382-44-3
diisobutyl(3,3-dimethylbut-1-en-1-yl)alane

: 201230-82-2
carbon monoxide

: 622-37-7
Phenyl azide

: 17767-01-0
4,4-Dimethylpent-2-enanilid

Guidance literature:: With palladium diacetate; XPhos; In tetrahydrofuran; hexane; at 80 ℃; for 16h; under 7500.75 Torr; Inert atmosphere; Sealed tube; Autoclave;
DOI:10.1016/j.jcat.2020.01.017

Reference yield:

: 630-19-3
pivalaldehyde

: 367508-00-7
N-Phenyl(diphenylphosphono)acetamide

: 17767-01-0
(E)-N-Phenyl-4,4-dimethyl-2-pentenoamide

: (Z)-N-Phenyl-4,4-dimethyl-2-pentenoamide

Guidance literature:: N-Phenyl(diphenylphosphono)acetamide; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.333333h;

pivalaldehyde; In tetrahydrofuran; at -78 - 10 ℃; for 2.5h; Title compound not separated from byproducts;
DOI:10.1055/s-2001-16072

Reference yield:

: 5326-87-4
N-(phenyl)bromoacetamide

: 17767-01-0
(E)-N-Phenyl-4,4-dimethyl-2-pentenoamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₃N / CH₂Cl₂

2.1: NaHMDS / tetrahydrofuran / 0.33 h / -78 °C

2.2: tetrahydrofuran / 2.5 h / -78 - 10 °C

With sodium hexamethyldisilazane; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2001-16072