(S)-benzyl (1-(1,2-dimethylhydrazinyl)-1-oxo-3-phenylpropan-2-yl)carbamate

Base Information

Chemical Name:(S)-benzyl (1-(1,2-dimethylhydrazinyl)-1-oxo-3-phenylpropan-2-yl)carbamate
CAS No.:1043922-50-4
Molecular Formula:C₁₉H₂₃N₃O₃
Molecular Weight:341.41
Hs Code.:

Synonyms:(S)-benzyl (1-(1,2-dimethylhydrazinyl)-1-oxo-3-phenylpropan-2-yl)carbamate

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Chemical Property of (S)-benzyl (1-(1,2-dimethylhydrazinyl)-1-oxo-3-phenylpropan-2-yl)carbamate

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Technology Process of (S)-benzyl (1-(1,2-dimethylhydrazinyl)-1-oxo-3-phenylpropan-2-yl)carbamate

There total 3 articles about (S)-benzyl (1-(1,2-dimethylhydrazinyl)-1-oxo-3-phenylpropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1161-13-3
N-Cbz-L-Phe

: 306-37-6
N,N'-Dimethylhydrazine dihydrochloride

: 1043922-50-4
(S)-benzyl (1-(1,2-dimethylhydrazinyl)-1-oxo-3-phenylpropan-2-yl)carbamate

Guidance literature:: N-Cbz-L-Phe; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -25 ℃;

N,N'-Dimethylhydrazine dihydrochloride; With sodium hydroxide; In tetrahydrofuran; water; at -25 - 20 ℃; for 2h;
DOI:10.1002/anie.200705858

Reference yield:

: 52641-32-4
N-benzyloxycarbonyl-L-phenylalanyl chloride

: 306-37-6
N,N'-Dimethylhydrazine dihydrochloride

: 1043922-50-4
(S)-benzyl (1-(1,2-dimethylhydrazinyl)-1-oxo-3-phenylpropan-2-yl)carbamate

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at -25 - 20 ℃;
DOI:10.1021/jm101272p

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 1043922-50-4
(S)-benzyl (1-(1,2-dimethylhydrazinyl)-1-oxo-3-phenylpropan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / -25 °C

2: sodium hydroxide / tetrahydrofuran; water / -25 - 20 °C

With 4-methyl-morpholine; sodium hydroxide; isobutyl chloroformate; In tetrahydrofuran; water;
DOI:10.1021/jm101272p