Silane, (1,1-dimethylethyl)[(1-ethoxycyclopropyl)oxy]dimethyl- (9CI)

Base Information

• Chemical Name: Silane, (1,1-dimethylethyl)[(1-ethoxycyclopropyl)oxy]dimethyl- (9CI)
• CAS No.: 117726-73-5
• Molecular Formula: C11H24 O2 Si
• Molecular Weight: 216.396
• Mol file: 117726-73-5.mol

Synonyms:Silane,(1,1-dimethylethyl)[(1-ethoxycyclopropyl)oxy]dimethyl- (9CI)

Chemical Property of Silane, (1,1-dimethylethyl)[(1-ethoxycyclopropyl)oxy]dimethyl- (9CI)

Chemical Property:

• PSA: 18.46000
• LogP: 3.53480

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Silane, (1,1-dimethylethyl)[(1-ethoxycyclopropyl)oxy]dimethyl- (9CI)

There total 1 articles about Silane, (1,1-dimethylethyl)[(1-ethoxycyclopropyl)oxy]dimethyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-ethoxycarbonyethylzinc iodide (104089-16-9) + tert-butyldimethylsilyl chloride (18162-48-6) → 1-Ethoxy-1-(tert-butyldimethylsiloxy)cyclopropan (117726-73-5)

Guidance literature:

In tetrahydrofuran; N,N-dimethyl acetamide; at 60 ℃; for 12h; Yield given;

Reference yield: 83.0%

1-Ethoxy-1-(tert-butyldimethylsiloxy)cyclopropan (117726-73-5) + 4-chloro-benzoyl chloride (122-01-0) → ethyl 4-(4-chlorophenyl)-4-oxobutanoate (53503-49-4)

Guidance literature:

(PhCO)PdCl(PPh₃)2*(CH₂Cl₂); In chloroform; at 90 - 100 ℃; for 24h;

DOI:10.1016/S0040-4039(01)89016-X

Reference yield: 59.0%

carbon monoxide (201230-82-2) + 1-Ethoxy-1-(tert-butyldimethylsiloxy)cyclopropan (117726-73-5) → 4-oxopimelate (6317-49-3)

Guidance literature:

bis-triphenylphosphine-palladium(II) chloride; In chloroform; at 60 ℃; under 760 Torr;

DOI:10.1016/S0040-4020(01)86434-6

upstream raw materials:

2-ethoxycarbonyethylzinc iodide

tert-butyldimethylsilyl chloride

Downstream raw materials:

4-oxopimelate

ethyl 4-(4-chlorophenyl)-4-oxobutanoate

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