2-(3-amino-4-methoxybenzylsulfanyl)-8-ethyl-9-methyl-6-morpholino-9H-purine

Base Information

Chemical Name:2-(3-amino-4-methoxybenzylsulfanyl)-8-ethyl-9-methyl-6-morpholino-9H-purine
CAS No.:1253847-02-7
Molecular Formula:C₂₀H₂₆N₆O₂S
Molecular Weight:414.531
Hs Code.:

Synonyms:2-(3-amino-4-methoxybenzylsulfanyl)-8-ethyl-9-methyl-6-morpholino-9H-purine

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Chemical Property of 2-(3-amino-4-methoxybenzylsulfanyl)-8-ethyl-9-methyl-6-morpholino-9H-purine

Chemical Property:

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Technology Process of 2-(3-amino-4-methoxybenzylsulfanyl)-8-ethyl-9-methyl-6-morpholino-9H-purine

There total 8 articles about 2-(3-amino-4-methoxybenzylsulfanyl)-8-ethyl-9-methyl-6-morpholino-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1253848-91-7
8-ethyl-9-methyl-6-morpholino-2-(3-nitro-4-methoxybenzylsulfanyl)-9H-purine

: 1253847-02-7
2-(3-amino-4-methoxybenzylsulfanyl)-8-ethyl-9-methyl-6-morpholino-9H-purine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; dichloromethane; for 18h; under 760.051 Torr;

Reference yield:

: 869119-60-8
4-chloro-2-(4-methoxybenzylsulfanyl)-6-methylaminopyrimidine

: 1253847-02-7
2-(3-amino-4-methoxybenzylsulfanyl)-8-ethyl-9-methyl-6-morpholino-9H-purine

Guidance literature:: Multi-step reaction with 5 steps

1.1: 80 °C

2.1: sodium nitrite; acetic acid / water / 5 h / 20 °C

2.3: 4 h / 760.05 Torr

3.1: methanol / 3 h / 20 °C

4.1: trifluoroacetic acid / methoxybenzene / 80 °C

4.2: Cooling with ice

5.1: hydrogen / palladium on activated charcoal / dichloromethane; methanol / 18 h / 760.05 Torr

With hydrogen; acetic acid; trifluoroacetic acid; sodium nitrite; palladium on activated charcoal; In methanol; dichloromethane; water; methoxybenzene;

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1253847-02-7
2-(3-amino-4-methoxybenzylsulfanyl)-8-ethyl-9-methyl-6-morpholino-9H-purine

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / N,N-dimethyl-formamide / 1.75 h / 100 °C

2.1: trichlorophosphate; N,N-dimethyl-aniline / 1.5 h / 100 °C

3.1: methanol / 20 °C

4.1: 80 °C

5.1: sodium nitrite; acetic acid / water / 5 h / 20 °C

5.3: 4 h / 760.05 Torr

6.1: methanol / 3 h / 20 °C

7.1: trifluoroacetic acid / methoxybenzene / 80 °C

7.2: Cooling with ice

8.1: hydrogen / palladium on activated charcoal / dichloromethane; methanol / 18 h / 760.05 Torr

With hydrogen; acetic acid; N,N-dimethyl-aniline; triethylamine; trifluoroacetic acid; sodium nitrite; trichlorophosphate; palladium on activated charcoal; In methanol; dichloromethane; water; methoxybenzene; N,N-dimethyl-formamide;