[PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(allyl alcohol)]BF₄

Base Information

Chemical Name:[PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(allyl alcohol)]BF₄
CAS No.:199284-80-5
Molecular Formula:BF₄*C₃₂H₄₉N₂OPt
Molecular Weight:759.638
Hs Code.:

[PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(allyl alcohol)]BF<sub>4</sub>

Synonyms:[PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(allyl alcohol)]BF₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(allyl alcohol)]BF₄

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Technology Process of [PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(allyl alcohol)]BF₄

There total 2 articles about [PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(allyl alcohol)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 14104-20-2
silver tetrafluoroborate

: 199284-91-8
[PtCl(Me)(diacetyl bis(2,6-diisopropylphenylimine))]

: 107-18-6
allyl alcohol

: 199284-80-5
[Pt(Me)(diacetyl bis(2,6-diisopropylphenylimine))(allyl alcohol)](BF₄)

Guidance literature:: In dichloromethane; byproducts: AgCl; mixing AgBF4 and excess of allyl alcohol, addn. of Pt-complex at 273 K, stirring for 48 h at room temp.; filtration off of AgCl (Celite), concn., crystn. on addn. of MePh and standing at 277 K, washing (MePh, pentane), drying (vac.); NMR spectroscopy;
DOI:10.1021/om970428f

Reference yield:

: 1,4-di(2,6-diisopropylphenyl)-2,3-dimethyl-1,4-diazabutadiene

: 199284-80-5
[Pt(Me)(diacetyl bis(2,6-diisopropylphenylimine))(allyl alcohol)](BF₄)

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: dichloromethane

In diethyl ether; dichloromethane;
DOI:10.1021/om970428f

Reference yield: 70.0%

: 199284-80-5
[PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(allyl alcohol)]BF₄

: 691894-19-6
[PtMe(N,N'-(1,2-dimethyl-1,2-ethanediylidene)bis(2,6-diisopropylaniline)))(allyl alcohol)]

Guidance literature:: With KOH; In methanol; soln. of KOH in methanol was added to stirred suspn. of Pt complex in methanol kept in ice bath; mixt. was stirred for 15 min; septd.; washed (cold methanol); dried (vac.); elem. anal.;
DOI:10.1021/om049968k