bis(triphenylphosphoranylidene)ammonium chloropentacarbonylmolybdate

Base Information

Chemical Name:bis(triphenylphosphoranylidene)ammonium chloropentacarbonylmolybdate
CAS No.:39048-41-4
Molecular Formula:C₅ClMoO₅*C₃₆H₃₀NP₂
Molecular Weight:810.033
Hs Code.:

Synonyms:bis(triphenylphosphoranylidene)ammonium chloropentacarbonylmolybdate

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Chemical Property of bis(triphenylphosphoranylidene)ammonium chloropentacarbonylmolybdate

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Technology Process of bis(triphenylphosphoranylidene)ammonium chloropentacarbonylmolybdate

There total 1 articles about bis(triphenylphosphoranylidene)ammonium chloropentacarbonylmolybdate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 21050-13-5
bis(triphenylphosphine)iminium chloride

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 39048-41-4
bis(triphenylphosphoranylidene)ammonium chloropentacarbonylmolybdate

Guidance literature:: In 1,2-dimethoxyethane; refluxing (4 h); filtering, pptn. on hexane addn., decanting, crystn. on repeated hexane addn., filtering, washing (hexane), drying (vac.);
DOI:10.1021/om970202c

Reference yield: 90.0%

: 39048-41-4
bis(triphenylphosphoranylidene)ammonium chloropentacarbonylmolybdate

: 2966-50-9
silver trifluoroacetate

: 76107-33-0
[((C₆H₅)3P)2N]⁽¹⁺⁾*[Mo(CO)5OOCCF₃]^(1-)=[((C₆H₅)3P)2N][Mo(CO)5OOCCF₃]

Guidance literature:: In dichloromethane; byproducts: AgCl; 10 min; filtered under N2, evapd. in vac., recrystd. from THF/hexane at -10°C;
DOI:10.1021/ja00392a026

Reference yield: 90.0%

: 39048-41-4
bis(triphenylphosphoranylidene)ammonium chloropentacarbonylmolybdate

: 563-63-3
silver(I) acetate

: 76107-32-9
[((C₆H₅)3P)2N]⁽¹⁺⁾*[Mo(CO)5(OCOCH₃)]^(1-)=[((C₆H₅)3P)2N][Mo(CO)5(OCOCH₃)]

Guidance literature:: In dichloromethane; byproducts: AgCl; 10 min; filtered under N2, evapd. in vac., recrystd. from THF/hexane at -10°C, elem. anal.;
DOI:10.1021/ja00392a026