4-amino-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}-4-oxobutanoic acid

Base Information

Chemical Name:4-amino-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}-4-oxobutanoic acid
CAS No.:1356599-49-9
Molecular Formula:C₂₆H₂₆N₂O₆
Molecular Weight:462.502
Hs Code.:

Synonyms:4-amino-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}-4-oxobutanoic acid

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Chemical Property of 4-amino-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}-4-oxobutanoic acid

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Technology Process of 4-amino-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}-4-oxobutanoic acid

There total 7 articles about 4-amino-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}-4-oxobutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.05%

: 1356601-66-5
methyl 3-cyano-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

: 1356599-49-9
4-amino-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}-4-oxobutanoic acid

Guidance literature:: methyl 3-cyano-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate; With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 2h;

With hydrogenchloride; In water; at 20 ℃; pH=6;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1356599-49-9
4-amino-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}-4-oxobutanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium acetate; acetic acid / 0.08 h / 20 °C

1.2: 3 h / 20 - 80 °C

2.1: potassium carbonate / acetonitrile / 0.08 h / 20 °C

2.2: 5 h / 20 - 80 °C

3.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 4 h / 0 - 20 °C

4.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C

4.2: 20 °C / pH 6

With tributylphosphine; water; sodium acetate; potassium carbonate; acetic acid; sodium hydroxide; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; toluene; acetonitrile;

Reference yield:

: 17315-86-5
2-(4-hydroxybenzylidene)malonic acid diethyl ester

: 1356599-49-9
4-amino-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}-4-oxobutanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol / 2 h / 70 °C

2.1: methanesulfonic acid / 1 h / Reflux

3.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 4 h / 0 - 20 °C

4.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C

4.2: 20 °C / pH 6

With methanesulfonic acid; tributylphosphine; water; sodium hydroxide; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; toluene;