6-[3-chloro-4-(3-hydroxy-propoxy)-phenyl]-4,5-dihydro-2H-pyridazin-3-one

Base Information

Chemical Name:6-[3-chloro-4-(3-hydroxy-propoxy)-phenyl]-4,5-dihydro-2H-pyridazin-3-one
CAS No.:141775-72-6
Molecular Formula:C₁₃H₁₅ClN₂O₃
Molecular Weight:282.727
Hs Code.:

Synonyms:6-[3-chloro-4-(3-hydroxy-propoxy)-phenyl]-4,5-dihydro-2H-pyridazin-3-one

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Chemical Property of 6-[3-chloro-4-(3-hydroxy-propoxy)-phenyl]-4,5-dihydro-2H-pyridazin-3-one

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Technology Process of 6-[3-chloro-4-(3-hydroxy-propoxy)-phenyl]-4,5-dihydro-2H-pyridazin-3-one

There total 1 articles about 6-[3-chloro-4-(3-hydroxy-propoxy)-phenyl]-4,5-dihydro-2H-pyridazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33821-94-2
3-(tetrahydro-2H-pyran-2-yloxy)propyl bromide

: 584-08-7
potassium carbonate

: 56872-24-3
6-(3-Chloro-4-hydroxyphenyl)-4,5-dihydro-3(2H)-pyridazinone

: 141775-72-6
6-[3-chloro-4-(3-hydroxy-propoxy)-phenyl]-4,5-dihydro-2H-pyridazin-3-one

Guidance literature:: With p-toluenesulfonic acid monohydrate; In methanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield: 33.0%

: 141775-72-6
6-[3-chloro-4-(3-hydroxy-propoxy)-phenyl]-4,5-dihydro-2H-pyridazin-3-one

: 623-05-2
(4-hydroxyphenyl)methanol

: 890042-58-7
6-{3-chloro-4-[3-(4-hydroxy-benzyloxy)-propoxy]-phenyl}-4,5-dihydro-2H-pyridazin-3-one

Guidance literature:: With ytterbium(III) triflate; In acetonitrile; for 4h; Heating / reflux;

Reference yield:

: 141775-72-6
6-[3-chloro-4-(3-hydroxy-propoxy)-phenyl]-4,5-dihydro-2H-pyridazin-3-one

: 3233-32-7
hydroquinone monoacetate

: 705290-37-5
acetic acid 4-{3-[2-chloro-4-(6-oxo-1,4,5,6-tetrahydro-pyridazin-3-yl)-phenoxy]-propoxy}phenyl ester

Guidance literature:: 6-[3-chloro-4-(3-hydroxy-propoxy)-phenyl]-4,5-dihydro-2H-pyridazin-3-one; hydroquinone monoacetate; With polystyrene supported triphenylphosphine resin; In dichloromethane; at -10 ℃; for 0.166667h;

With di-isopropyl azodicarboxylate; In dichloromethane; at 20 ℃; for 16h;