cis-3,4-dihydroxy-trans-3,5-dimethyl-1-(phenylsulfonyl)cyclohexene 3,4-acetonide

Base Information

Chemical Name:cis-3,4-dihydroxy-trans-3,5-dimethyl-1-(phenylsulfonyl)cyclohexene 3,4-acetonide
CAS No.:82769-83-3
Molecular Formula:C₁₇H₂₂O₄S
Molecular Weight:322.425
Hs Code.:

Synonyms:cis-3,4-dihydroxy-trans-3,5-dimethyl-1-(phenylsulfonyl)cyclohexene 3,4-acetonide

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Chemical Property of cis-3,4-dihydroxy-trans-3,5-dimethyl-1-(phenylsulfonyl)cyclohexene 3,4-acetonide

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Technology Process of cis-3,4-dihydroxy-trans-3,5-dimethyl-1-(phenylsulfonyl)cyclohexene 3,4-acetonide

There total 2 articles about cis-3,4-dihydroxy-trans-3,5-dimethyl-1-(phenylsulfonyl)cyclohexene 3,4-acetonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 82769-82-2
trans,cis-3,5-dimethyl-1-(phenylsulfonyl)-trans,cis,cis-2,3,4-trihydroxycyclohexane 3,4-acetonide

: 82769-83-3
cis-3,4-dihydroxy-trans-3,5-dimethyl-1-(phenylsulfonyl)cyclohexene 3,4-acetonide

Guidance literature:: With trichlorophosphate; In pyridine; at 110 ℃; for 3h;
DOI:10.1021/ja00385a030

Reference yield:

: 81939-86-8
trans,cis-3,5-dimethyl-1-phenylthio-trans,cis,cis-2,3,4-trihydroxycyclohexane 3,4-acetonide

: 82769-83-3
cis-3,4-dihydroxy-trans-3,5-dimethyl-1-(phenylsulfonyl)cyclohexene 3,4-acetonide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / Ambient temperature

2: 91 percent / phosphorus oxychloride / pyridine / 3 h / 110 °C

With 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In pyridine; dichloromethane;
DOI:10.1021/ja00385a030

Reference yield: 89.5%

: 82769-83-3
cis-3,4-dihydroxy-trans-3,5-dimethyl-1-(phenylsulfonyl)cyclohexene 3,4-acetonide

: 82769-89-9
anti-N,N-dimethyl-1-acetylcyclopropanecarboxamine dimethylhydrazone

: 82769-90-2
(1'RS,2'RS,3'SR,4'SR,6'RS)-N,N-dimethyl-1-<1-(2,2-dimethyl-1,1-diazanediyl)-2-(2',3'-dihydroxy-2',4'-dimethyl-6'-(phenylsulfonyl)cyclohexyl)ethyl>cyclopropanecarboxamide 2',3'-acetonide

Guidance literature:: With Diethoxy-methyl-(6-amino-hexylaminomethyl)-silan; In tetrahydrofuran; 1.) -78 deg C -> 0 deg C, 10 min, 2.) 0 deg C, 1 h;
DOI:10.1021/ja00385a030