Carbonic acid allyl ester 1-cyano-5-(2-methoxy-6-nitro-phenyl)-4-oxo-pentyl ester

Base Information

Chemical Name:Carbonic acid allyl ester 1-cyano-5-(2-methoxy-6-nitro-phenyl)-4-oxo-pentyl ester
CAS No.:124832-36-6
Molecular Formula:C₁₇H₁₈N₂O₇
Molecular Weight:362.339
Hs Code.:

Synonyms:Carbonic acid allyl ester 1-cyano-5-(2-methoxy-6-nitro-phenyl)-4-oxo-pentyl ester

Suppliers and Price of Carbonic acid allyl ester 1-cyano-5-(2-methoxy-6-nitro-phenyl)-4-oxo-pentyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbonic acid allyl ester 1-cyano-5-(2-methoxy-6-nitro-phenyl)-4-oxo-pentyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of Carbonic acid allyl ester 1-cyano-5-(2-methoxy-6-nitro-phenyl)-4-oxo-pentyl ester

There total 4 articles about Carbonic acid allyl ester 1-cyano-5-(2-methoxy-6-nitro-phenyl)-4-oxo-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 143-33-9,25596-52-5
sodium cyanide

: 136552-17-5
5-(2-Methoxy-6-nitro-phenyl)-4-oxo-pentanal

: 2937-50-0
Allyl chloroformate

: 124832-36-6
Carbonic acid allyl ester 1-cyano-5-(2-methoxy-6-nitro-phenyl)-4-oxo-pentyl ester

Guidance literature:: DOI:10.1016/S0040-4039(00)99254-2

Reference yield:

: 20876-28-2
2-(2-methoxy-6-nitrophenyl)acetic acid

: 124832-36-6
Carbonic acid allyl ester 1-cyano-5-(2-methoxy-6-nitro-phenyl)-4-oxo-pentyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1) SOCl₂ / 2) TiCl₄

2: 89 percent / 9-BBN, H₂O₂, NaOH

3: 84 percent / DMSO, ClCOCOCl, Et₃N / CH₂Cl₂

4: 94 percent

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; thionyl chloride; oxalyl dichloride; dihydrogen peroxide; dimethyl sulfoxide; triethylamine; titanium tetrachloride; In dichloromethane;
DOI:10.1016/S0040-4039(00)99254-2

Reference yield:

: 124832-33-3
1-(2-Methoxy-6-nitro-phenyl)-pent-4-en-2-one

: 124832-36-6
Carbonic acid allyl ester 1-cyano-5-(2-methoxy-6-nitro-phenyl)-4-oxo-pentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / 9-BBN, H₂O₂, NaOH

2: 84 percent / DMSO, ClCOCOCl, Et₃N / CH₂Cl₂

3: 94 percent

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; oxalyl dichloride; dihydrogen peroxide; dimethyl sulfoxide; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)99254-2