Technology Process of C14H18FNO2
There total 5 articles about C14H18FNO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
carbonochloridic acid 1-chloro-ethyl ester;
In
dichloromethane;
at 20 ℃;
for 2h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium; iodine / tetrahydrofuran / 1 h / Reflux
1.2: 3 h / 20 °C / Reflux
2.1: sulfuric acid / 12 h / 90 °C
3.1: diethylamino-sulfur trifluoride / dichloromethane / 3 h / -78 - 20 °C / Inert atmosphere
4.1: carbonochloridic acid 1-chloro-ethyl ester / dichloromethane / 2 h / 20 °C / Inert atmosphere
With
carbonochloridic acid 1-chloro-ethyl ester; diethylamino-sulfur trifluoride; sulfuric acid; iodine; magnesium;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium; iodine / tetrahydrofuran / 1 h / Reflux
1.2: 3 h / 20 °C / Reflux
2.1: sulfuric acid / 12 h / 90 °C
3.1: diethylamino-sulfur trifluoride / dichloromethane / 3 h / -78 - 20 °C / Inert atmosphere
4.1: carbonochloridic acid 1-chloro-ethyl ester / dichloromethane / 2 h / 20 °C / Inert atmosphere
With
carbonochloridic acid 1-chloro-ethyl ester; diethylamino-sulfur trifluoride; sulfuric acid; iodine; magnesium;
In
tetrahydrofuran; dichloromethane;