11-(4-METHOXYPHENYL)-3,3-DIMETHYL-2,3,4,5,10,11-HEXAHYDRO-1H-DIBENZO[B,E][1,4]DIAZEPIN-1-ONE

Base Information

Chemical Name:11-(4-METHOXYPHENYL)-3,3-DIMETHYL-2,3,4,5,10,11-HEXAHYDRO-1H-DIBENZO[B,E][1,4]DIAZEPIN-1-ONE
CAS No.:82408-02-4
Molecular Formula:C₂₂H₂₄N₂O₂
Molecular Weight:348.445
Hs Code.:
Mol file:82408-02-4.mol

Synonyms:3,3-dimethyl-2,3,4,5,10,11-hexahydro-11-[(4-methoxy)phenyl]-1H-dibenzo[b,e][1,4]diazepin-1-one

Suppliers and Price of 11-(4-METHOXYPHENYL)-3,3-DIMETHYL-2,3,4,5,10,11-HEXAHYDRO-1H-DIBENZO[B,E][1,4]DIAZEPIN-1-ONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
11-(4-METHOXYPHENYL)-3,3-DIMETHYL-2,3,4,5,10,11-HEXAHYDRO-1H-DIBENZO(B,E)(1,4)DIAZEPIN-1-ONE 95.00%
5MG
$ 687.35

American Custom Chemicals Corporation
11-(4-METHOXYPHENYL)-3,3-DIMETHYL-2,3,4,5,10,11-HEXAHYDRO-1H-DIBENZO(B,E)(1,4)DIAZEPIN-1-ONE 95.00%
10MG
$ 679.14

American Custom Chemicals Corporation
11-(4-METHOXYPHENYL)-3,3-DIMETHYL-2,3,4,5,10,11-HEXAHYDRO-1H-DIBENZO(B,E)(1,4)DIAZEPIN-1-ONE 95.00%
1MG
$ 647.61

Total 0 raw suppliers

Chemical Property of 11-(4-METHOXYPHENYL)-3,3-DIMETHYL-2,3,4,5,10,11-HEXAHYDRO-1H-DIBENZO[B,E][1,4]DIAZEPIN-1-ONE

Chemical Property:

Purity/Quality:: 11-(4-METHOXYPHENYL)-3,3-DIMETHYL-2,3,4,5,10,11-HEXAHYDRO-1H-DIBENZO(B,E)(1,4)DIAZEPIN-1-ONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 11-(4-METHOXYPHENYL)-3,3-DIMETHYL-2,3,4,5,10,11-HEXAHYDRO-1H-DIBENZO[B,E][1,4]DIAZEPIN-1-ONE

There total 8 articles about 11-(4-METHOXYPHENYL)-3,3-DIMETHYL-2,3,4,5,10,11-HEXAHYDRO-1H-DIBENZO[B,E][1,4]DIAZEPIN-1-ONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 123-11-5
4-methoxy-benzaldehyde

: 126-81-8
dimedone

: 95-54-5
1,2-diamino-benzene

: 82408-02-4
3,3-dimethyl-2,3,4,5,10,11-hexahydro-11-[(4-methoxy)phenyl]-1H-dibenzo[b,e][1,4]diazepin-1-one

Guidance literature:: With silica-supported nickel oxide nanocomposites; In ethanol; at 70 ℃; for 0.166667h; Microwave irradiation; Green chemistry;
DOI:10.1039/c6nj04013f

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 39222-69-0
3-[(2-aminophenyl)amino]-5,5-dimethylcyclohex-2-en-1-one

: 82408-02-4
3,3-dimethyl-2,3,4,5,10,11-hexahydro-11-[(4-methoxy)phenyl]-1H-dibenzo[b,e][1,4]diazepin-1-one

Guidance literature:: In isopropyl alcohol; Heating;
DOI:10.1007/s10593-005-0098-3

Reference yield:

: 3471-13-4
dimedone

: 82408-02-4
3,3-dimethyl-2,3,4,5,10,11-hexahydro-11-[(4-methoxy)phenyl]-1H-dibenzo[b,e][1,4]diazepin-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH / propan-2-ol / 0.67 h / Heating

2: propan-2-ol / Heating

With acetic acid; In isopropyl alcohol;
DOI:10.1007/s10593-005-0098-3