3, 5-dimethyl-4-(4-methoxyphenyl)-1,4,7,8-tetrahydrodipyrazolo[3,4-b;4’,3’-e]pyridine

Base Information

Chemical Name:3, 5-dimethyl-4-(4-methoxyphenyl)-1,4,7,8-tetrahydrodipyrazolo[3,4-b;4’,3’-e]pyridine
CAS No.:1346446-00-1
Molecular Formula:C₁₆H₁₇N₅O
Molecular Weight:295.344
Hs Code.:

Synonyms:3, 5-dimethyl-4-(4-methoxyphenyl)-1,4,7,8-tetrahydrodipyrazolo[3,4-b;4’,3’-e]pyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3, 5-dimethyl-4-(4-methoxyphenyl)-1,4,7,8-tetrahydrodipyrazolo[3,4-b;4’,3’-e]pyridine

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Technology Process of 3, 5-dimethyl-4-(4-methoxyphenyl)-1,4,7,8-tetrahydrodipyrazolo[3,4-b;4’,3’-e]pyridine

There total 3 articles about 3, 5-dimethyl-4-(4-methoxyphenyl)-1,4,7,8-tetrahydrodipyrazolo[3,4-b;4’,3’-e]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 141-97-9
ethyl acetoacetate

: 123-11-5
4-methoxy-benzaldehyde

: 1346446-00-1
3, 5-dimethyl-4-(4-methoxyphenyl)-1,4,7,8-tetrahydrodipyrazolo[3,4-b;4’,3’-e]pyridine

Guidance literature:: With triethanolamine; ammonium acetate; sodium acetate; hydrazine hydrate; for 0.05h; Reagent/catalyst; Catalytic behavior; Microwave irradiation;
DOI:10.1007/s13738-021-02178-z

Reference yield: 93.0%

: 123-11-5
4-methoxy-benzaldehyde

: 108-26-9
3-methyl-2-pyrazoline-5-one

: 1346446-00-1
3, 5-dimethyl-4-(4-methoxyphenyl)-1,4,7,8-tetrahydrodipyrazolo[3,4-b;4’,3’-e]pyridine

Guidance literature:: With phospho sulphonic acid; ammonium acetate; In neat (no solvent); at 70 ℃; for 0.333333h; under 760.051 Torr; Microwave irradiation; Green chemistry;
DOI:10.1002/jhet.4241

Reference yield: 90.0%

: 123-11-5
4-methoxy-benzaldehyde

: 105-45-3
acetoacetic acid methyl ester

: 1346446-00-1
3, 5-dimethyl-4-(4-methoxyphenyl)-1,4,7,8-tetrahydrodipyrazolo[3,4-b;4’,3’-e]pyridine

Guidance literature:: With ammonium acetate; Cl₄Co^(2-)*2Cl^(1-)*4C₅H₁₄NO⁽¹⁺⁾; hydrazine; In water; at 20 ℃; for 0.333333h;
DOI:10.1016/j.molliq.2020.112722